C₃₁H₃₂BrNO₄

Base Information

Chemical Name:C₃₁H₃₂BrNO₄
CAS No.:1463522-90-8
Molecular Formula:C₃₁H₃₂BrNO₄
Molecular Weight:562.503
Hs Code.:

C<sub>31</sub>H<sub>32</sub>BrNO<sub>4</sub>

Synonyms:C₃₁H₃₂BrNO₄

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Chemical Property of C₃₁H₃₂BrNO₄

Chemical Property:

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Technology Process of C₃₁H₃₂BrNO₄

There total 6 articles about C₃₁H₃₂BrNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 20769-85-1
2-bromoisobutyric acid bromide

: 1463523-04-7
2-(6-(ethyl(prop-2-yn-1-yl)amino)-4,4-diphenyl-4H-benzo[d][1,3]dioxin-2-yl)ethanol

: 1463522-90-8
C₃₁H₃₂BrNO₄

Guidance literature:: With dmap; triethylamine; In dichloromethane; at -10 - 20 ℃; Inert atmosphere;
DOI:10.1039/c3cc44799e

Reference yield:

: 89-57-6
5-Aminosalicylic Acid

: 1463522-90-8
C₃₁H₃₂BrNO₄

Guidance literature:: Multi-step reaction with 6 steps

1: Acidic conditions

2: triethylamine

3: Neutral conditions

4: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux

5: sodium carbonate; tetra-(n-butyl)ammonium iodide / acetone; toluene / 2.5 h / Reflux

6: dmap; triethylamine / dichloromethane / -10 - 20 °C / Inert atmosphere

With dmap; lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; sodium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; acetone; toluene; 2: |Grignard Reaction;
DOI:10.1039/c3cc44799e

Reference yield:

: C₂₄H₂₅NO₃

: 1463522-90-8
C₃₁H₃₂BrNO₄

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; tetra-(n-butyl)ammonium iodide / acetone; toluene / 2.5 h / Reflux

2: dmap; triethylamine / dichloromethane / -10 - 20 °C / Inert atmosphere

With dmap; tetra-(n-butyl)ammonium iodide; sodium carbonate; triethylamine; In dichloromethane; acetone; toluene;
DOI:10.1039/c3cc44799e