4-(4-chlorophenyl)-2-(ethoxycarbonyl)methyl-5-phenyl-2H-[1,2,3]triazole

Base Information

Chemical Name:4-(4-chlorophenyl)-2-(ethoxycarbonyl)methyl-5-phenyl-2H-[1,2,3]triazole
CAS No.:1024656-40-3
Molecular Formula:C₁₈H₁₆ClN₃O₂
Molecular Weight:341.797
Hs Code.:

Synonyms:4-(4-chlorophenyl)-2-(ethoxycarbonyl)methyl-5-phenyl-2H-[1,2,3]triazole

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Chemical Property of 4-(4-chlorophenyl)-2-(ethoxycarbonyl)methyl-5-phenyl-2H-[1,2,3]triazole

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Technology Process of 4-(4-chlorophenyl)-2-(ethoxycarbonyl)methyl-5-phenyl-2H-[1,2,3]triazole

There total 2 articles about 4-(4-chlorophenyl)-2-(ethoxycarbonyl)methyl-5-phenyl-2H-[1,2,3]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 105-36-2
ethyl bromoacetate

: 120106-67-4,148101-05-7
4-(4-chlorophenyl)-5-phenyl-1H(2H)-[1,2,3]triazole

: 1024656-40-3
4-(4-chlorophenyl)-2-(ethoxycarbonyl)methyl-5-phenyl-2H-[1,2,3]triazole

: 1248827-40-8
C₁₈H₁₆ClN₃O₂

: 1248827-38-4
C₁₈H₁₆ClN₃O₂

Guidance literature:: 4-(4-chlorophenyl)-5-phenyl-1H(2H)-[1,2,3]triazole; With tetrabutylammomium bromide; potassium carbonate; potassium hydroxide; In acetonitrile; at 20 ℃; for 0.0833333h;

ethyl bromoacetate; In acetonitrile; for 5h; Reflux;
DOI:10.3998/ark.5550190.0011.210

Reference yield:

: 1024656-40-3
4-(4-chlorophenyl)-2-(ethoxycarbonyl)methyl-5-phenyl-2H-[1,2,3]triazole

Guidance literature:

Reference yield: 70.0%

: 4319-49-7
1-aminomorpholine

: 1024656-40-3
4-(4-chlorophenyl)-2-(ethoxycarbonyl)methyl-5-phenyl-2H-[1,2,3]triazole

: 4-(4-chlorophenyl)-5-phenyl-2-(morpholin-4-ylcarbamoyl)methyl-2H-[1,2,3]triazole

Guidance literature:: 1-aminomorpholine; With trimethylaluminum; In n-heptane; dichloromethane; at 20 ℃; Inert atmosphere;

4-(4-chlorophenyl)-2-(ethoxycarbonyl)methyl-5-phenyl-2H-[1,2,3]triazole; In n-heptane; dichloromethane; at 20 - 40 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; In n-heptane; dichloromethane; water; at 0 - 40 ℃; for 0.5h;
DOI:10.3998/ark.5550190.0011.210