methyl 2-methoxycarbonyl-3-ethoxycarbonyl-4-(3-fluoroanilinocarbonylhydrazono)pentanoate

Base Information

Chemical Name:methyl 2-methoxycarbonyl-3-ethoxycarbonyl-4-(3-fluoroanilinocarbonylhydrazono)pentanoate
CAS No.:350620-58-5
Molecular Formula:C₁₈H₂₂FN₃O₇
Molecular Weight:411.387
Hs Code.:

Synonyms:methyl 2-methoxycarbonyl-3-ethoxycarbonyl-4-(3-fluoroanilinocarbonylhydrazono)pentanoate

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Chemical Property of methyl 2-methoxycarbonyl-3-ethoxycarbonyl-4-(3-fluoroanilinocarbonylhydrazono)pentanoate

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Technology Process of methyl 2-methoxycarbonyl-3-ethoxycarbonyl-4-(3-fluoroanilinocarbonylhydrazono)pentanoate

There total 1 articles about methyl 2-methoxycarbonyl-3-ethoxycarbonyl-4-(3-fluoroanilinocarbonylhydrazono)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 108-59-8
malonic acid dimethyl ester

: C₁₃H₁₄FN₃O₃

: 350620-58-5
methyl 2-methoxycarbonyl-3-ethoxycarbonyl-4-(3-fluoroanilinocarbonylhydrazono)pentanoate

Guidance literature:: With sodium methylate; In tetrahydrofuran; at 20 ℃; for 0.1h;
DOI:10.1039/b009189h

Reference yield: 60.0%

: 350620-58-5
methyl 2-methoxycarbonyl-3-ethoxycarbonyl-4-(3-fluoroanilinocarbonylhydrazono)pentanoate

: 63160-41-8
1-aminocarbonyl-3-methyl-4-methoxycarbonyl-1,2-diaza-1,3-diene

: 350620-59-6
3-ethyl-4,4,5-trimethyl-2(3-fluoroanilinocarbonyl)hydrazono-6-aminocarbonyl-hydrazonoheptane-3,4,4,5-tetracarboxylate

Guidance literature:: With sodium methylate; In tetrahydrofuran; at 20 ℃; for 8.5h;
DOI:10.1039/b009189h

Reference yield:

: 350620-58-5
methyl 2-methoxycarbonyl-3-ethoxycarbonyl-4-(3-fluoroanilinocarbonylhydrazono)pentanoate

: N-(7-aminocarbonylamino-3,8-dimethyl-4-ethoxycarbonyl-9-methoxycarbonyl-1,6-dioxo-2,7-diazaspiro[4.4]nona-3,8-dien-2-yl)-N'-3-fluorophenylurea

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / CH₃ONa / tetrahydrofuran / 8.5 h / 20 °C

2: 74 percent / CH₃ONa / methanol / 1.5 h / 20 °C

With sodium methylate; In tetrahydrofuran; methanol;
DOI:10.1039/b009189h