3-ethyl-4,4,5-trimethyl-2(3-fluoroanilinocarbonyl)hydrazono-6-aminocarbonyl-hydrazonoheptane-3,4,4,5-tetracarboxylate

Base Information

Chemical Name:3-ethyl-4,4,5-trimethyl-2(3-fluoroanilinocarbonyl)hydrazono-6-aminocarbonyl-hydrazonoheptane-3,4,4,5-tetracarboxylate
CAS No.:350620-59-6
Molecular Formula:C₂₄H₃₁FN₆O₁₀
Molecular Weight:582.543
Hs Code.:

Synonyms:3-ethyl-4,4,5-trimethyl-2(3-fluoroanilinocarbonyl)hydrazono-6-aminocarbonyl-hydrazonoheptane-3,4,4,5-tetracarboxylate

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Chemical Property of 3-ethyl-4,4,5-trimethyl-2(3-fluoroanilinocarbonyl)hydrazono-6-aminocarbonyl-hydrazonoheptane-3,4,4,5-tetracarboxylate

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Technology Process of 3-ethyl-4,4,5-trimethyl-2(3-fluoroanilinocarbonyl)hydrazono-6-aminocarbonyl-hydrazonoheptane-3,4,4,5-tetracarboxylate

There total 3 articles about 3-ethyl-4,4,5-trimethyl-2(3-fluoroanilinocarbonyl)hydrazono-6-aminocarbonyl-hydrazonoheptane-3,4,4,5-tetracarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 350620-58-5
methyl 2-methoxycarbonyl-3-ethoxycarbonyl-4-(3-fluoroanilinocarbonylhydrazono)pentanoate

: 63160-41-8
1-aminocarbonyl-3-methyl-4-methoxycarbonyl-1,2-diaza-1,3-diene

: 350620-59-6
3-ethyl-4,4,5-trimethyl-2(3-fluoroanilinocarbonyl)hydrazono-6-aminocarbonyl-hydrazonoheptane-3,4,4,5-tetracarboxylate

Guidance literature:: With sodium methylate; In tetrahydrofuran; at 20 ℃; for 8.5h;
DOI:10.1039/b009189h

Reference yield:

: 108-59-8
malonic acid dimethyl ester

: 350620-59-6
3-ethyl-4,4,5-trimethyl-2(3-fluoroanilinocarbonyl)hydrazono-6-aminocarbonyl-hydrazonoheptane-3,4,4,5-tetracarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / CH₃ONa / tetrahydrofuran / 0.1 h / 20 °C

2: 60 percent / CH₃ONa / tetrahydrofuran / 8.5 h / 20 °C

With sodium methylate; In tetrahydrofuran;
DOI:10.1039/b009189h

Reference yield:

: C₁₃H₁₄FN₃O₃

: 350620-59-6
3-ethyl-4,4,5-trimethyl-2(3-fluoroanilinocarbonyl)hydrazono-6-aminocarbonyl-hydrazonoheptane-3,4,4,5-tetracarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / CH₃ONa / tetrahydrofuran / 0.1 h / 20 °C

2: 60 percent / CH₃ONa / tetrahydrofuran / 8.5 h / 20 °C

With sodium methylate; In tetrahydrofuran;
DOI:10.1039/b009189h