5-(tricyclo<3.3.1.1^3,7>dec-1-yl)-dihydro-3-(dimethylaminomethyl)-5-phenylfuran-2(3H)-one

Base Information

• Chemical Name: 5-(tricyclo<3.3.1.1^3,7>dec-1-yl)-dihydro-3-(dimethylaminomethyl)-5-phenylfuran-2(3H)-one
• CAS No.: 777821-90-6
• Molecular Formula: C₂₃H₃₁NO₂
• Molecular Weight: 353.505

Synonyms:5-(tricyclo<3.3.1.1^3,7>dec-1-yl)-dihydro-3-(dimethylaminomethyl)-5-phenylfuran-2(3H)-one

Chemical Property of 5-(tricyclo<3.3.1.1^3,7>dec-1-yl)-dihydro-3-(dimethylaminomethyl)-5-phenylfuran-2(3H)-one

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Technology Process of 5-(tricyclo<3.3.1.1^3,7>dec-1-yl)-dihydro-3-(dimethylaminomethyl)-5-phenylfuran-2(3H)-one

There total 2 articles about 5-(tricyclo<3.3.1.1^3,7>dec-1-yl)-dihydro-3-(dimethylaminomethyl)-5-phenylfuran-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

acide 5-(tricyclo<3.3.1.13,7>dec-1-yl)-tetrahydro-2-oxo-5-phenylfurane-3-carboxylique (134753-57-4) → 5-(tricyclo<3.3.1.13,7>dec-1-yl)-dihydro-3-methylene-5-phenylfuran-2(3H)-one (97839-58-2) + 5-(tricyclo<3.3.1.13,7>dec-1-yl)-dihydro-3-(dimethylaminomethyl)-5-phenylfuran-2(3H)-one (777821-90-6)

Guidance literature:

With formaldehyd; dimethyl amine; In ethanol; at 0 ℃; for 30h;

DOI:10.1016/0223-5234(91)90213-7

Reference yield: 56.0%

acide 5-(tricyclo<3.3.1.13,7>dec-1-yl)-tetrahydro-2-oxo-5-phenylfurane-3-carboxylique (134753-57-4) + dimethyl amine (124-40-3) → 5-(tricyclo<3.3.1.13,7>dec-1-yl)-dihydro-3-methylene-5-phenylfuran-2(3H)-one (97839-58-2) + 5-(tricyclo<3.3.1.13,7>dec-1-yl)-dihydro-3-(dimethylaminomethyl)-5-phenylfuran-2(3H)-one (777821-90-6)

Guidance literature:

With formaldehyd; In ethanol; at 0 ℃; for 30h;

DOI:10.1016/0223-5234(91)90213-7

Reference yield:

5-(tricyclo<3.3.1.13,7>dec-1-yl)-dihydro-3-(dimethylaminomethyl)-5-phenylfuran-2(3H)-one (777821-90-6) → 1-(tricyclo<3.3.1.13,7>dec-1-yl)-3-(dimethylaminomethyl)-1-phenylbutane-1,4-diol (134753-59-6)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 5h; Yield given; Heating;

DOI:10.1016/0223-5234(91)90213-7

upstream raw materials:

acide 5-(tricyclo<3.3.1.1^3,7>dec-1-yl)-tetrahydro-2-oxo-5-phenylfurane-3-carboxylique

dimethyl amine

Downstream raw materials:

1-(tricyclo<3.3.1.1^3,7>dec-1-yl)-3-(dimethylaminomethyl)-1-phenylbutane-1,4-diol

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