3,5-dibutoxycarbonylphenyl glycinamide

Base Information

Chemical Name:3,5-dibutoxycarbonylphenyl glycinamide
CAS No.:852355-45-4
Molecular Formula:C₁₈H₂₆N₂O₅
Molecular Weight:350.415
Hs Code.:

Synonyms:3,5-dibutoxycarbonylphenyl glycinamide

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Chemical Property of 3,5-dibutoxycarbonylphenyl glycinamide

Chemical Property:

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Technology Process of 3,5-dibutoxycarbonylphenyl glycinamide

There total 4 articles about 3,5-dibutoxycarbonylphenyl glycinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 852355-44-3
3,5-dibutoxycarbonylphenyl bromoacetamide

: 852355-45-4
3,5-dibutoxycarbonylphenyl glycinamide

Guidance literature:: With ammonia; In tetrahydrofuran; methanol; for 4h;
DOI:10.1021/ol050341n

Reference yield:

: 10552-75-7
dibutyl 5-nitroisophthalate

: 852355-45-4
3,5-dibutoxycarbonylphenyl glycinamide

Guidance literature:: Multi-step reaction with 3 steps

1: 51.3 g / ammonium formate / Pd/C / methanol; tetrahydrofuran / 1.5 h / Heating

2: 98 percent / Na₂CO₃ / acetonitrile / 2 h

3: 78 percent / NH₃ / tetrahydrofuran; methanol / 4 h

With ammonia; ammonium formate; sodium carbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ol050341n

Reference yield:

: 618-88-2
5-nitrobenzene-1,3-dicarboxylic acid

: 852355-45-4
3,5-dibutoxycarbonylphenyl glycinamide

Guidance literature:: Multi-step reaction with 4 steps

1: p-toluenesulfonic acid monohydrate / benzene / Heating

2: 51.3 g / ammonium formate / Pd/C / methanol; tetrahydrofuran / 1.5 h / Heating

3: 98 percent / Na₂CO₃ / acetonitrile / 2 h

4: 78 percent / NH₃ / tetrahydrofuran; methanol / 4 h

With ammonia; ammonium formate; sodium carbonate; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; acetonitrile; benzene;
DOI:10.1021/ol050341n