dibutyl 5-nitroisophthalate

Base Information

Chemical Name:dibutyl 5-nitroisophthalate
CAS No.:10552-75-7
Molecular Formula:C₁₆H₂₁NO₆
Molecular Weight:323.346
Hs Code.:

Synonyms:dibutyl 5-nitroisophthalate

Suppliers and Price of dibutyl 5-nitroisophthalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibutyl 5-nitroisophthalate

Chemical Property:

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Technology Process of dibutyl 5-nitroisophthalate

There total 1 articles about dibutyl 5-nitroisophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 618-88-2
5-nitrobenzene-1,3-dicarboxylic acid

: 71-36-3
butan-1-ol

: 10552-75-7
dibutyl 5-nitroisophthalate

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Heating;
DOI:10.1021/ol050341n

Reference yield:

: 10552-75-7
dibutyl 5-nitroisophthalate

: 60166-93-0,60208-45-9,62883-00-5
Iopamidol

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogen; 5%-palladium/activated carbon / 50 - 70 °C

2: sodium methylate / methanol / 55 - 60 °C

3: sulfuric acid; Iodine monochloride / water / 70 - 90 °C

4: N,N-dimethyl acetamide / 1 h / 90 - 95 °C

5: N,N-dimethyl acetamide / 18 h / 30 - 35 °C / Inert atmosphere; Large scale

6: sodium hydroxide; water / N,N-dimethyl acetamide / Large scale

With sulfuric acid; 5%-palladium/activated carbon; water; hydrogen; sodium methylate; Iodine monochloride; sodium hydroxide; In methanol; N,N-dimethyl acetamide; water;

Reference yield:

: 10552-75-7
dibutyl 5-nitroisophthalate

: 25351-79-5
5-amino-isophthalic acid dibutyl ester

Guidance literature:: With ammonium formate; palladium on activated charcoal; In tetrahydrofuran; methanol; for 1.5h; Heating;
DOI:10.1021/ol050341n