(S)-3-(4-(allyloxy)-2,3,5,6-tetrafluorophenyl)-2-(tert-butoxycarbonylamino)propanoic acid

Base Information

Chemical Name:(S)-3-(4-(allyloxy)-2,3,5,6-tetrafluorophenyl)-2-(tert-butoxycarbonylamino)propanoic acid
CAS No.:1259967-10-6
Molecular Formula:C₁₇H₁₉F₄NO₅
Molecular Weight:393.335
Hs Code.:

Synonyms:(S)-3-(4-(allyloxy)-2,3,5,6-tetrafluorophenyl)-2-(tert-butoxycarbonylamino)propanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-(4-(allyloxy)-2,3,5,6-tetrafluorophenyl)-2-(tert-butoxycarbonylamino)propanoic acid

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Technology Process of (S)-3-(4-(allyloxy)-2,3,5,6-tetrafluorophenyl)-2-(tert-butoxycarbonylamino)propanoic acid

There total 1 articles about (S)-3-(4-(allyloxy)-2,3,5,6-tetrafluorophenyl)-2-(tert-butoxycarbonylamino)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 107-18-6
allyl alcohol

: 136207-26-6,34702-60-8
(S)-2-((tert-butoxycarbonyl)amino)-3-(perfluorophenyl)propanoic acid

: 1259967-10-6
(S)-3-(4-(allyloxy)-2,3,5,6-tetrafluorophenyl)-2-(tert-butoxycarbonylamino)propanoic acid

Guidance literature:: With sodium; at 0 - 90 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol102610q

Reference yield:

: 1259967-10-6
(S)-3-(4-(allyloxy)-2,3,5,6-tetrafluorophenyl)-2-(tert-butoxycarbonylamino)propanoic acid

: C₁₂H₁₁F₄NO₃

Guidance literature:: With triethylsilane; trifluoroacetic acid; In water; at 20 ℃; for 1h;
DOI:10.1021/ol102610q

Reference yield:

: 1259967-10-6
(S)-3-(4-(allyloxy)-2,3,5,6-tetrafluorophenyl)-2-(tert-butoxycarbonylamino)propanoic acid

: 1259967-11-7
(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-(allyloxy)-2,3,5,6-tetrafluorophenyl)propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylsilane; trifluoroacetic acid / water / 1 h / 20 °C

2: sodium carbonate / water; acetonitrile / 2.5 h / 20 °C

With triethylsilane; sodium carbonate; trifluoroacetic acid; In water; acetonitrile;
DOI:10.1021/ol102610q