1,1-dimethylethyl {2-[[(1R,2R)-2-hydroxy-1-methyl-2-phenylethyl](methyl)amino]-2-oxoethyl}methylcarbamate

Base Information

Chemical Name:1,1-dimethylethyl {2-[[(1R,2R)-2-hydroxy-1-methyl-2-phenylethyl](methyl)amino]-2-oxoethyl}methylcarbamate
CAS No.:1093865-11-2
Molecular Formula:C₁₈H₂₈N₂O₄
Molecular Weight:336.431
Hs Code.:

Synonyms:1,1-dimethylethyl {2-[[(1R,2R)-2-hydroxy-1-methyl-2-phenylethyl](methyl)amino]-2-oxoethyl}methylcarbamate

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Chemical Property of 1,1-dimethylethyl {2-[[(1R,2R)-2-hydroxy-1-methyl-2-phenylethyl](methyl)amino]-2-oxoethyl}methylcarbamate

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Technology Process of 1,1-dimethylethyl {2-[[(1R,2R)-2-hydroxy-1-methyl-2-phenylethyl](methyl)amino]-2-oxoethyl}methylcarbamate

There total 3 articles about 1,1-dimethylethyl {2-[[(1R,2R)-2-hydroxy-1-methyl-2-phenylethyl](methyl)amino]-2-oxoethyl}methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.2%

: 4530-20-5
BOC-glycine

: 321-97-1,7009-81-6,90-83-5,6912-63-6
(1R,2R)-pseudoephedrine

: 541-41-3
chloroformic acid ethyl ester

: 1093865-11-2
1,1-dimethylethyl {2-[[(1R,2R)-2-hydroxy-1-methyl-2-phenylethyl](methyl)amino]-2-oxoethyl}methylcarbamate

Guidance literature:: BOC-glycine; chloroformic acid ethyl ester; With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 2.16667h;

(1R,2R)-pseudoephedrine; In tetrahydrofuran; at 20 ℃; for 18h;

Reference yield:

: 321-97-1,7009-81-6,90-83-5,6912-63-6
(1R,2R)-pseudoephedrine

: C₁₁H₁₉NO₆

: 1093865-11-2
1,1-dimethylethyl {2-[[(1R,2R)-2-hydroxy-1-methyl-2-phenylethyl](methyl)amino]-2-oxoethyl}methylcarbamate

Guidance literature:: In tetrahydrofuran; at 20 ℃;

Reference yield:

: 13734-36-6
N-(tert-butoxycarbonyl)sarcosine

: 1093865-11-2
1,1-dimethylethyl {2-[[(1R,2R)-2-hydroxy-1-methyl-2-phenylethyl](methyl)amino]-2-oxoethyl}methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 2.17 h / 0 - 20 °C

2: tetrahydrofuran / 20 °C

With triethylamine; In tetrahydrofuran;