(trans)-1-[N-[(2-mercaptocyclohexyl)carbonyl]-L-alanyl]-L-proline, monolithium salt

Base Information

• Chemical Name: (trans)-1-[N-[(2-mercaptocyclohexyl)carbonyl]-L-alanyl]-L-proline, monolithium salt
• CAS No.: 104264-63-3
• Molecular Formula: C₁₅H₂₃N₂O₄S*Li
• Molecular Weight: 334.366

Synonyms:(trans)-1-[N-[(2-mercaptocyclohexyl)carbonyl]-L-alanyl]-L-proline, monolithium salt

Chemical Property of (trans)-1-[N-[(2-mercaptocyclohexyl)carbonyl]-L-alanyl]-L-proline, monolithium salt

Chemical Property:

Purity/Quality:

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Technology Process of (trans)-1-[N-[(2-mercaptocyclohexyl)carbonyl]-L-alanyl]-L-proline, monolithium salt

There total 1 articles about (trans)-1-[N-[(2-mercaptocyclohexyl)carbonyl]-L-alanyl]-L-proline, monolithium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(trans)-1-[N-[[[(4-methoxyphenyl)methyl]thio]cyclohexylcarbonyl]-L-alanyl]-L-proline + 2,2'-oxybis(2-methyl-propane) (6163-66-2) → (trans)-1-[N-[(2-mercaptocyclohexyl)carbonyl]-L-alanyl]-L-proline, monolithium salt (104264-63-3)

Guidance literature:

With lithium hydroxide; In chloroform; mercury(II) diacetate; water; acetic acid; ethyl acetate; toluene;

Reference yield:

(trans)-1-[N-[(2-mercaptocyclohexyl)carbonyl]-L-alanyl]-L-proline + (trans)-1-[N-[(2-mercaptocyclohexyl)carbonyl]-L-alanyl]-L-proline, monolithium salt (104264-63-3) + benzoyl chloride (98-88-4) → (trans)-1-[N-[[(2-benzoylthio)cyclohexyl]carbonyl]-L-alanyl]-L-proline

Guidance literature:

With triethylamine; In dichloromethane; chloroform; ethyl acetate;

upstream raw materials:

2,2'-oxybis(2-methyl-propane)

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