dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate-2,2-dioxide

Base Information

Chemical Name:dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate-2,2-dioxide
CAS No.:864236-32-8
Molecular Formula:C₁₇H₁₇NO₆S
Molecular Weight:363.391
Hs Code.:

Synonyms:dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate-2,2-dioxide

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Chemical Property of dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate-2,2-dioxide

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Technology Process of dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate-2,2-dioxide

There total 3 articles about dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate-2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 864236-31-7
dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate

: 864236-32-8
dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate-2,2-dioxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/jo050480i

Reference yield:

: N-benzoyl-2-methyl-1,3-thiazolidine-4-carboxylic acid

: 864236-32-8
dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate-2,2-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / acetic anhydride / 4 h / Heating

2: 93 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

With acetic anhydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo050480i

Reference yield:

: 762-42-5
dimethyl acetylenedicarboxylate

: 864236-32-8
dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate-2,2-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / acetic anhydride / 4 h / Heating

2: 93 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

With acetic anhydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo050480i