dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate

Base Information

Chemical Name:dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate
CAS No.:864236-31-7
Molecular Formula:C₁₇H₁₇NO₄S
Molecular Weight:331.392
Hs Code.:

Synonyms:dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate

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Chemical Property of dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate

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Technology Process of dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate

There total 1 articles about dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: N-benzoyl-2-methyl-1,3-thiazolidine-4-carboxylic acid

: 762-42-5
dimethyl acetylenedicarboxylate

: 864236-31-7
dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate

Guidance literature:: With acetic anhydride; for 4h; Heating;
DOI:10.1021/jo050480i

Reference yield: 93.0%

: 864236-31-7
dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate

: 864236-32-8
dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate-2,2-dioxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/jo050480i

Reference yield:

: 864236-31-7
dimethyl 3-methyl-5-phenyl-1H,3H-pyrrolo[1,2-c]thiazole-6,7-dicarboxylate

: 864236-44-2
dimethyl 2-methyl-5-phenyl-1-vinyl-1H-pyrrole-3,4-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

2: 45 percent / tetrahydrothiophene 1,1-dioxide / 1.5 h / 260 °C

With 3-chloro-benzenecarboperoxoic acid; In sulfolane; dichloromethane;
DOI:10.1021/jo050480i