8-methoxycarbonyloct-1-yl 2-acetamido-4-O-(tetra-O-acetyl-β-D-galactopyranosyl)-6-O-benzoyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:8-methoxycarbonyloct-1-yl 2-acetamido-4-O-(tetra-O-acetyl-β-D-galactopyranosyl)-6-O-benzoyl-2-deoxy-β-D-glucopyranoside
CAS No.:173097-00-2
Molecular Formula:C₃₉H₅₅NO₁₈
Molecular Weight:825.862
Hs Code.:

Synonyms:8-methoxycarbonyloct-1-yl 2-acetamido-4-O-(tetra-O-acetyl-β-D-galactopyranosyl)-6-O-benzoyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of 8-methoxycarbonyloct-1-yl 2-acetamido-4-O-(tetra-O-acetyl-β-D-galactopyranosyl)-6-O-benzoyl-2-deoxy-β-D-glucopyranoside

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Technology Process of 8-methoxycarbonyloct-1-yl 2-acetamido-4-O-(tetra-O-acetyl-β-D-galactopyranosyl)-6-O-benzoyl-2-deoxy-β-D-glucopyranoside

There total 5 articles about 8-methoxycarbonyloct-1-yl 2-acetamido-4-O-(tetra-O-acetyl-β-D-galactopyranosyl)-6-O-benzoyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 98-88-4
benzoyl chloride

: 173096-99-6
8-methoxycarbonyloct-1-yl 2-acetamido-4-O-(tetra-O-acetyl-β-D-galactopyranosyl)-2-deoxy-β-D-glucopyranoside

: 173097-00-2
8-methoxycarbonyloct-1-yl 2-acetamido-4-O-(tetra-O-acetyl-β-D-galactopyranosyl)-6-O-benzoyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane;
DOI:10.1016/0008-6215(95)00235-L

Reference yield:

: 97205-24-8
8-methoxycarbonyloct-1-yl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 173097-00-2
8-methoxycarbonyloct-1-yl 2-acetamido-4-O-(tetra-O-acetyl-β-D-galactopyranosyl)-6-O-benzoyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: sodium cyanoborohydride, 3A molecular sieves, methyl orange / tetrahydrofuran

2: 4A molecular sieves / CH₂Cl₂ / 3 h / -30 °C

3: 96 percent / H₂ / 5percent Pd/C / methanol / 3 h

4: 87 percent / pyridine / CH₂Cl₂

With pyridine; 3 A molecular sieve; 4 A molecular sieve; hydrogen; methyl orange; sodium cyanoborohydride; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/0008-6215(95)00235-L

Reference yield:

: 97205-25-9
8-methoxycarbonyloct-1-yl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 173097-00-2
8-methoxycarbonyloct-1-yl 2-acetamido-4-O-(tetra-O-acetyl-β-D-galactopyranosyl)-6-O-benzoyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 4A molecular sieves / CH₂Cl₂ / 3 h / -30 °C

2: 96 percent / H₂ / 5percent Pd/C / methanol / 3 h

3: 87 percent / pyridine / CH₂Cl₂

With pyridine; 4 A molecular sieve; hydrogen; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/0008-6215(95)00235-L