3-(2,6-dimethylphenyl)-11-((9-(pyridin-2-yl)-9H-carbazol-2-yl)oxy)imidazo[1,2-f]phenanthridine

Base Information

Chemical Name:3-(2,6-dimethylphenyl)-11-((9-(pyridin-2-yl)-9H-carbazol-2-yl)oxy)imidazo[1,2-f]phenanthridine
CAS No.:1395093-69-2
Molecular Formula:C₄₀H₂₈N₄O
Molecular Weight:580.689
Hs Code.:

Synonyms:3-(2,6-dimethylphenyl)-11-((9-(pyridin-2-yl)-9H-carbazol-2-yl)oxy)imidazo[1,2-f]phenanthridine

Suppliers and Price of 3-(2,6-dimethylphenyl)-11-((9-(pyridin-2-yl)-9H-carbazol-2-yl)oxy)imidazo[1,2-f]phenanthridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2,6-dimethylphenyl)-11-((9-(pyridin-2-yl)-9H-carbazol-2-yl)oxy)imidazo[1,2-f]phenanthridine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-(2,6-dimethylphenyl)-11-((9-(pyridin-2-yl)-9H-carbazol-2-yl)oxy)imidazo[1,2-f]phenanthridine

There total 6 articles about 3-(2,6-dimethylphenyl)-11-((9-(pyridin-2-yl)-9H-carbazol-2-yl)oxy)imidazo[1,2-f]phenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1352932-32-1
2-bromo-9-(pyridin-2-yl)-9H-carbazole 3-Br

: 1395093-66-9
3-(2,6-dimethylphenyl)imidazo[1,2-f]phenanthridin-11-ol

: 1395093-69-2
3-(2,6-dimethylphenyl)-11-((9-(pyridin-2-yl)-9H-carbazol-2-yl)oxy)imidazo[1,2-f]phenanthridine

Guidance literature:: With 2-Picolinic acid; copper(l) iodide; potassium phosphate monohydrate; In dimethyl sulfoxide; at 150 ℃; for 24.3333h;

Reference yield:

: 191171-55-8
2-anilineboronic acid pinacol ester

: 1395093-69-2
3-(2,6-dimethylphenyl)-11-((9-(pyridin-2-yl)-9H-carbazol-2-yl)oxy)imidazo[1,2-f]phenanthridine

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium phosphate monohydrate / bis-triphenylphosphine-palladium(II) chloride / toluene; water / 15.5 h / Inert atmosphere

2.1: isopropyl alcohol / 24 h / Reflux

2.2: 16 h / 60 °C / Reflux

3.1: boron tribromide / dichloromethane / -78 - 20 °C

4.1: copper(l) iodide; potassium phosphate monohydrate; 2-Picolinic acid / dimethyl sulfoxide / 24.33 h / 150 °C

With 2-Picolinic acid; copper(l) iodide; potassium phosphate monohydrate; boron tribromide; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol; toluene;

Reference yield:

: 138642-47-4
2-bromo-5-methoxybenzonitrile

: 1395093-69-2
3-(2,6-dimethylphenyl)-11-((9-(pyridin-2-yl)-9H-carbazol-2-yl)oxy)imidazo[1,2-f]phenanthridine

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium phosphate monohydrate / bis-triphenylphosphine-palladium(II) chloride / toluene; water / 15.5 h / Inert atmosphere

2.1: isopropyl alcohol / 24 h / Reflux

2.2: 16 h / 60 °C / Reflux

3.1: boron tribromide / dichloromethane / -78 - 20 °C

4.1: copper(l) iodide; potassium phosphate monohydrate; 2-Picolinic acid / dimethyl sulfoxide / 24.33 h / 150 °C

With 2-Picolinic acid; copper(l) iodide; potassium phosphate monohydrate; boron tribromide; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol; toluene;