1-Propanone, 3-(diethylamino)-1-(2,3,4,5-tetrahydro-1,6-benzodioxocin-8-yl)-, hydrochloride

Base Information

Chemical Name:1-Propanone, 3-(diethylamino)-1-(2,3,4,5-tetrahydro-1,6-benzodioxocin-8-yl)-, hydrochloride
CAS No.:132412-85-2
Molecular Formula:C17H26ClNO3
Molecular Weight:327.8462
Hs Code.:
DSSTox Substance ID:DTXSID00157543

Synonyms:1-Propanone, 3-(diethylamino)-1-(2,3,4,5-tetrahydro-1,6-benzodioxocin-8-yl)-, hydrochloride;3-(Diethylamino)-1-(2,3,4,5-tetrahydro-1,6-benzodioxocin-8-yl)-1-propanone hydrochloride;132412-85-2;DTXSID00157543;LS-122868

Suppliers and Price of 1-Propanone, 3-(diethylamino)-1-(2,3,4,5-tetrahydro-1,6-benzodioxocin-8-yl)-, hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Propanone, 3-(diethylamino)-1-(2,3,4,5-tetrahydro-1,6-benzodioxocin-8-yl)-, hydrochloride

Chemical Property:

Vapor Pressure:1.35E-07mmHg at 25°C
Boiling Point:429.9°C at 760 mmHg
Flash Point:213.8°C
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:327.1601214
Heavy Atom Count:22
Complexity:317

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)CCC(=O)C1=CC2=C(C=C1)OCCCCO2.Cl

Technology Process of 1-Propanone, 3-(diethylamino)-1-(2,3,4,5-tetrahydro-1,6-benzodioxocin-8-yl)-, hydrochloride

There total 2 articles about 1-Propanone, 3-(diethylamino)-1-(2,3,4,5-tetrahydro-1,6-benzodioxocin-8-yl)-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 660-68-4
diethyl amine hydrochloride

: 127119-37-3
1-(2,3,4,5-Tetrahydro-benzo[b][1,4]dioxocin-8-yl)-ethanone

: 132412-85-2
3-Diethylamino-1-(2,3,4,5-tetrahydro-benzo[b][1,4]dioxocin-8-yl)-propan-1-one; hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; for 10h; Heating;
DOI:10.1007/BF00768387

Reference yield:

: 7124-91-6
2,3,4,5-Tetrahydro-benzo[b][1,4]dioxocin

: 132412-85-2
3-Diethylamino-1-(2,3,4,5-tetrahydro-benzo[b][1,4]dioxocin-8-yl)-propan-1-one; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / AlCl₃ / CH₂Cl₂ / 2 h / 20 °C

2: 52 percent / conc. HCl / ethanol / 10 h / Heating

With hydrogenchloride; aluminium trichloride; In ethanol; dichloromethane;
DOI:10.1007/BF00768387