trifluoro-methanesulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

Base Information

Chemical Name:trifluoro-methanesulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester
CAS No.:1207529-71-2
Molecular Formula:C₁₆H₁₆ClF₆NO₄S
Molecular Weight:467.817
Hs Code.:

Synonyms:trifluoro-methanesulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

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Chemical Property of trifluoro-methanesulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

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Technology Process of trifluoro-methanesulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

There total 4 articles about trifluoro-methanesulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 1207530-03-7
trans-2-chloro-N-(4-hydroxymethyl-cyclohexyl)-5-trifluoromethyl-benzamide

: 1207529-71-2
trifluoro-methanesulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 657-05-6
2-chloro-5-trifluoromethylbenzoyl chloride

: 1207529-71-2
trifluoro-methanesulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 1.83 h / 0 - 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere

2.2: 0 °C

3.1: pyridine / dichloromethane / 1 h / 0 °C

With pyridine; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 61367-07-5,61367-16-6,100707-54-8
trans-4-aminocyclohexylcarboxylic acid methyl ester hydrochloride

: 1207529-71-2
trifluoro-methanesulfonic acid trans-4-(2-chloro-5-trifluoromethyl-benzoylamino)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 1.83 h / 0 - 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere

2.2: 0 °C

3.1: pyridine / dichloromethane / 1 h / 0 °C

With pyridine; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;