C₄₅H₄₂O₇

Base Information

Chemical Name:C₄₅H₄₂O₇
CAS No.:1365537-69-4
Molecular Formula:C₄₅H₄₂O₇
Molecular Weight:694.824
Hs Code.:

C<sub>45</sub>H<sub>42</sub>O<sub>7</sub>

Synonyms:C₄₅H₄₂O₇

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Chemical Property of C₄₅H₄₂O₇

Chemical Property:

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Technology Process of C₄₅H₄₂O₇

There total 11 articles about C₄₅H₄₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₃₆O₇

: 100-39-0
benzyl bromide

: 1365537-69-4
C₄₅H₄₂O₇

Guidance literature:: C₃₈H₃₆O₇; With sodium hydride; In N,N-dimethyl-formamide; mineral oil;

benzyl bromide; In N,N-dimethyl-formamide; mineral oil; for 2.5h;
DOI:10.1016/j.tetlet.2012.01.054

Reference yield:

: C₃₈H₃₆O₇

: 1365537-69-4
C₄₅H₄₂O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: Dess-Martin periodane / dichloromethane; water / 2 h

2.1: aluminum isopropoxide; isopropyl alcohol / toluene / 1 h / 100 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil

3.2: 2.5 h

With aluminum isopropoxide; sodium hydride; Dess-Martin periodane; isopropyl alcohol; In dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil; 2.1: Meerwein-Ponndorf-Verley reduction;
DOI:10.1016/j.tetlet.2012.01.054

Reference yield:

: 1365537-42-3
C₃₈H₃₄O₇

: 1365537-69-4
C₄₅H₄₂O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / tetrahydrofuran; ethanol / 5.08 h / -40 - 0 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C

3.1: AD-mix-α; methanesulfonamide; water / tetrahydrofuran; tert-butyl alcohol / 16 h / 0 - 20 °C

4.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 0 °C

5.1: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 2 h / 65 °C

6.1: methanol; ammonia / 48 h / 20 °C

7.1: Dess-Martin periodane / dichloromethane; water / 2 h

8.1: aluminum isopropoxide; isopropyl alcohol / toluene / 1 h / 100 °C

9.1: sodium hydride / N,N-dimethyl-formamide; mineral oil

9.2: 2.5 h

With 1H-imidazole; methanol; sodium tetrahydroborate; methanesulfonamide; cerium(III) chloride heptahydrate; AD-mix-α; tetrabutyl ammonium fluoride; ammonia; water; pyridinium p-toluenesulfonate; aluminum isopropoxide; sodium hydride; Dess-Martin periodane; acetic acid; isopropyl alcohol; In tetrahydrofuran; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; mineral oil; tert-butyl alcohol; 3.1: Sharpless dihydroxylation / 8.1: Meerwein-Ponndorf-Verley reduction;
DOI:10.1016/j.tetlet.2012.01.054