2-Acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-D-xylo-hexopyranose

Base Information

Chemical Name:2-Acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-D-xylo-hexopyranose
CAS No.:136408-96-3
Molecular Formula:C₁₈H₂₇NO₇
Molecular Weight:369.415
Hs Code.:

Synonyms:2-Acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-D-xylo-hexopyranose

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Chemical Property of 2-Acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-D-xylo-hexopyranose

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Technology Process of 2-Acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-D-xylo-hexopyranose

There total 9 articles about 2-Acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-D-xylo-hexopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 136408-95-2
1-Propenyl-2-acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-α-D-xylo-hexopyranosid

: 136408-96-3
2-Acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-D-xylo-hexopyranose

Guidance literature:: With mercury dichloride; mercury(II) oxide; In water; acetone; for 1.5h;

Reference yield:

: 54400-75-8
allyl 2-acetamido-2-deoxy-α-D-glucopyranoside

: 136408-96-3
2-Acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-D-xylo-hexopyranose

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / CSA / acetonitrile / 0.5 h

2: 83 percent / 2,6-lutidine / acetonitrile / 16 h / Heating

3: 79 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 0 °C

4: 1) 5 N NaOH / 1) 5 deg C, 30 min., 2) 1 h

5: 75 percent / Bu₃SnH, AIBN / toluene / 110 °C

6: 1) 1,5,7-triazabicyclo<4.4.0>dec-5-ene, 2) HgO, HgCl₂ / 1) triphenylphosphan-rhodium chloride / 1) EtOH, H₂O, 10 h, reflux, 2) acetone, H₂O

With 2,6-dimethylpyridine; sodium hydroxide; 2,2'-azobis(isobutyronitrile); 3 A molecular sieve; camphor-10-sulfonic acid; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; tri-n-butyl-tin hydride; sodium cyanoborohydride; trifluoroacetic acid; mercury dichloride; mercury(II) oxide; triphenylphosphan-rhodium chloride; In tetrahydrofuran; toluene; acetonitrile;

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 136408-96-3
2-Acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-D-xylo-hexopyranose

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / CSA / acetonitrile / 0.5 h

2: 83 percent / 2,6-lutidine / acetonitrile / 16 h / Heating

3: 79 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 0 °C

4: 1) 5 N NaOH / 1) 5 deg C, 30 min., 2) 1 h

5: 75 percent / Bu₃SnH, AIBN / toluene / 110 °C

6: 1) 1,5,7-triazabicyclo<4.4.0>dec-5-ene, 2) HgO, HgCl₂ / 1) triphenylphosphan-rhodium chloride / 1) EtOH, H₂O, 10 h, reflux, 2) acetone, H₂O

With 2,6-dimethylpyridine; sodium hydroxide; 2,2'-azobis(isobutyronitrile); 3 A molecular sieve; camphor-10-sulfonic acid; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; tri-n-butyl-tin hydride; sodium cyanoborohydride; trifluoroacetic acid; mercury dichloride; mercury(II) oxide; triphenylphosphan-rhodium chloride; In tetrahydrofuran; toluene; acetonitrile;