1-Propenyl-2-acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-α-D-xylo-hexopyranosid

Base Information

Chemical Name:1-Propenyl-2-acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-α-D-xylo-hexopyranosid
CAS No.:136408-95-2
Molecular Formula:C₂₁H₃₁NO₇
Molecular Weight:409.48
Hs Code.:

Synonyms:1-Propenyl-2-acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-α-D-xylo-hexopyranosid

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Chemical Property of 1-Propenyl-2-acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-α-D-xylo-hexopyranosid

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Technology Process of 1-Propenyl-2-acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-α-D-xylo-hexopyranosid

There total 8 articles about 1-Propenyl-2-acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-α-D-xylo-hexopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 136408-94-1
Allyl-2-acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-α-D-xylo-hexopyranosid

: 136408-95-2
1-Propenyl-2-acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-α-D-xylo-hexopyranosid

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; for 4h; Heating;

Reference yield:

: 54400-75-8
allyl 2-acetamido-2-deoxy-α-D-glucopyranoside

: 136408-95-2
1-Propenyl-2-acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-α-D-xylo-hexopyranosid

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / CSA / acetonitrile / 0.5 h

2: 83 percent / 2,6-lutidine / acetonitrile / 16 h / Heating

3: 79 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 0 °C

4: 1) 5 N NaOH / 1) 5 deg C, 30 min., 2) 1 h

5: 75 percent / Bu₃SnH, AIBN / toluene / 110 °C

6: 86 percent / tert-BuOK / dimethylsulfoxide / 4 h / Heating

With 2,6-dimethylpyridine; sodium hydroxide; 2,2'-azobis(isobutyronitrile); 3 A molecular sieve; camphor-10-sulfonic acid; potassium tert-butylate; tri-n-butyl-tin hydride; sodium cyanoborohydride; trifluoroacetic acid; In tetrahydrofuran; dimethyl sulfoxide; toluene; acetonitrile;

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 136408-95-2
1-Propenyl-2-acetamido-2,4-didesoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-α-D-xylo-hexopyranosid

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / CSA / acetonitrile / 0.5 h

2: 83 percent / 2,6-lutidine / acetonitrile / 16 h / Heating

3: 79 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 0 °C

4: 1) 5 N NaOH / 1) 5 deg C, 30 min., 2) 1 h

5: 75 percent / Bu₃SnH, AIBN / toluene / 110 °C

6: 86 percent / tert-BuOK / dimethylsulfoxide / 4 h / Heating

With 2,6-dimethylpyridine; sodium hydroxide; 2,2'-azobis(isobutyronitrile); 3 A molecular sieve; camphor-10-sulfonic acid; potassium tert-butylate; tri-n-butyl-tin hydride; sodium cyanoborohydride; trifluoroacetic acid; In tetrahydrofuran; dimethyl sulfoxide; toluene; acetonitrile;