(S)-N-((1S)-1-(4-(2,4-diaminophenyl)pyridin-2-yl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

Base Information

Chemical Name:(S)-N-((1S)-1-(4-(2,4-diaminophenyl)pyridin-2-yl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide
CAS No.:1422387-14-1
Molecular Formula:C₁₉H₂₆N₄OS
Molecular Weight:358.508
Hs Code.:

Synonyms:(S)-N-((1S)-1-(4-(2,4-diaminophenyl)pyridin-2-yl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

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Chemical Property of (S)-N-((1S)-1-(4-(2,4-diaminophenyl)pyridin-2-yl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

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Technology Process of (S)-N-((1S)-1-(4-(2,4-diaminophenyl)pyridin-2-yl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

There total 3 articles about (S)-N-((1S)-1-(4-(2,4-diaminophenyl)pyridin-2-yl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1329167-88-5
(S)-N-((1S)-1-(4-(2-amino-4-nitrophenyl)pyridin-2-yl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

: 1422387-14-1
(S)-N-((1S)-1-(4-(2,4-diaminophenyl)pyridin-2-yl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

Guidance literature:: With ammonium chloride; zinc; In methanol; at 20 ℃; for 2h; Sealed tube;

Reference yield:

: 1329166-69-9
2‐(5,5‐dimethyl‐1,3,2‐dioxaborinan‐2‐yl)‐5‐nitroaniline

: 1422387-14-1
(S)-N-((1S)-1-(4-(2,4-diaminophenyl)pyridin-2-yl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium phosphate / water; dimethyl sulfoxide / 4 h / 90 °C / Inert atmosphere

2: zinc; ammonium chloride / methanol / 2 h / 20 °C / Sealed tube

With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; ammonium chloride; zinc; In methanol; water; dimethyl sulfoxide;

Reference yield:

: 10403-47-1
2-bromo 5-nitroaniline

: 1422387-14-1
(S)-N-((1S)-1-(4-(2,4-diaminophenyl)pyridin-2-yl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / dimethyl sulfoxide / 4.5 h / 80 °C / Inert atmosphere

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium phosphate / water; dimethyl sulfoxide / 4 h / 90 °C / Inert atmosphere

3: zinc; ammonium chloride / methanol / 2 h / 20 °C / Sealed tube

With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; ammonium chloride; zinc; In methanol; water; dimethyl sulfoxide;