(S)-methyl 3-amino-4-(2-(1-aminobut-3-enyl)pyridin-4-yl)phenylcarbamate

Base Information

Chemical Name:(S)-methyl 3-amino-4-(2-(1-aminobut-3-enyl)pyridin-4-yl)phenylcarbamate
CAS No.:1422423-29-7
Molecular Formula:C₁₇H₂₀N₄O₂
Molecular Weight:312.371
Hs Code.:

Synonyms:(S)-methyl 3-amino-4-(2-(1-aminobut-3-enyl)pyridin-4-yl)phenylcarbamate

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Chemical Property of (S)-methyl 3-amino-4-(2-(1-aminobut-3-enyl)pyridin-4-yl)phenylcarbamate

Chemical Property:

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Technology Process of (S)-methyl 3-amino-4-(2-(1-aminobut-3-enyl)pyridin-4-yl)phenylcarbamate

There total 5 articles about (S)-methyl 3-amino-4-(2-(1-aminobut-3-enyl)pyridin-4-yl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422387-15-2
methyl (3-amino-4-(2-((S)-1-((S)-1,1-dimethylethylsulfinamido)but-3-en-1-yl)pyridin-4-yl)phenyl)carbamate

: 1422423-29-7
(S)-methyl 3-amino-4-(2-(1-aminobut-3-enyl)pyridin-4-yl)phenylcarbamate

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃; for 2h;

Reference yield:

: 10403-47-1
2-bromo 5-nitroaniline

: 1422423-29-7
(S)-methyl 3-amino-4-(2-(1-aminobut-3-enyl)pyridin-4-yl)phenylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / dimethyl sulfoxide / 4.5 h / 80 °C / Inert atmosphere

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium phosphate / water; dimethyl sulfoxide / 4 h / 90 °C / Inert atmosphere

3: zinc; ammonium chloride / methanol / 2 h / 20 °C / Sealed tube

4: pyridine / dichloromethane / 2 h / -78 °C

5: hydrogenchloride / methanol; 1,4-dioxane / 2 h / 20 °C

With pyridine; hydrogenchloride; potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; ammonium chloride; zinc; In 1,4-dioxane; methanol; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 1329166-69-9
2‐(5,5‐dimethyl‐1,3,2‐dioxaborinan‐2‐yl)‐5‐nitroaniline

: 1422423-29-7
(S)-methyl 3-amino-4-(2-(1-aminobut-3-enyl)pyridin-4-yl)phenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium phosphate / water; dimethyl sulfoxide / 4 h / 90 °C / Inert atmosphere

2: zinc; ammonium chloride / methanol / 2 h / 20 °C / Sealed tube

3: pyridine / dichloromethane / 2 h / -78 °C

4: hydrogenchloride / methanol; 1,4-dioxane / 2 h / 20 °C

With pyridine; hydrogenchloride; potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; ammonium chloride; zinc; In 1,4-dioxane; methanol; dichloromethane; water; dimethyl sulfoxide;