N-<2-(3,4-Methylenedioxyphenyl)ethyl>-2'-bromo-5'-methoxyphenylacetamide

Base Information

Chemical Name:N-<2-(3,4-Methylenedioxyphenyl)ethyl>-2'-bromo-5'-methoxyphenylacetamide
CAS No.:86826-94-0
Molecular Formula:C₁₈H₁₈BrNO₄
Molecular Weight:392.249
Hs Code.:

Synonyms:N-<2-(3,4-Methylenedioxyphenyl)ethyl>-2'-bromo-5'-methoxyphenylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-(3,4-Methylenedioxyphenyl)ethyl>-2'-bromo-5'-methoxyphenylacetamide

Chemical Property:

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Technology Process of N-<2-(3,4-Methylenedioxyphenyl)ethyl>-2'-bromo-5'-methoxyphenylacetamide

There total 4 articles about N-<2-(3,4-Methylenedioxyphenyl)ethyl>-2'-bromo-5'-methoxyphenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 86826-93-9
2-(2-bromo-5-methoxyphenyl)acetic acid

: 1484-85-1
3,4-methylenedioxyphenylethylamine

: 86826-94-0
N-<2-(3,4-Methylenedioxyphenyl)ethyl>-2'-bromo-5'-methoxyphenylacetamide

Guidance literature:: at 180 ℃; for 3h;

Reference yield:

: 1798-09-0
m-methoxyphenylacetic acid

: 86826-94-0
N-<2-(3,4-Methylenedioxyphenyl)ethyl>-2'-bromo-5'-methoxyphenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / Br₂, NaOAc / acetic acid / 3 h / ice-bath

2: 87 percent / 3 h / 180 °C

With bromine; sodium acetate; In acetic acid;

Reference yield:

: 86826-93-9
2-(2-bromo-5-methoxyphenyl)acetic acid

: 86826-94-0
N-<2-(3,4-Methylenedioxyphenyl)ethyl>-2'-bromo-5'-methoxyphenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane

2: triethylamine / dichloromethane

With oxalyl dichloride; triethylamine; In dichloromethane;
DOI:10.1111/cbdd.13390