2-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-N-methoxy-N-methylbutanamide

Base Information

Chemical Name:2-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-N-methoxy-N-methylbutanamide
CAS No.:1453470-32-0
Molecular Formula:C₁₉H₃₃NO₄Si
Molecular Weight:367.561
Hs Code.:

Synonyms:2-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-N-methoxy-N-methylbutanamide

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Chemical Property of 2-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-N-methoxy-N-methylbutanamide

Chemical Property:

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Technology Process of 2-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-N-methoxy-N-methylbutanamide

There total 1 articles about 2-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-N-methoxy-N-methylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 1453470-32-0
2-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-N-methoxy-N-methylbutanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: silver(l) oxide; tetra-(n-butyl)ammonium iodide / dichloromethane / 30 h / 20 °C / Darkness

2.1: diisobutylaluminium hydride / tetrahydrofuran; n-heptane / 5 h / 20 °C

2.2: 20 °C

With tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; silver(l) oxide; In tetrahydrofuran; n-heptane; dichloromethane;
DOI:10.1021/ol402017x

Reference yield: 57.0%

: 1453470-32-0
2-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-N-methoxy-N-methylbutanamide

: 1826-67-1
vinyl magnesium bromide

: 1453470-40-0
4-(benzyloxy)-6-(tert-butyldimethylsilyloxy)hex-1-en-3-one

Guidance literature:: In tetrahydrofuran; diethyl ether; at -40 ℃; for 5h;
DOI:10.1021/ol402017x

Reference yield:

: 1453470-32-0
2-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-N-methoxy-N-methylbutanamide

: 1453470-56-8
C₂₉H₅₂O₅Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether / 5 h / -40 °C

2: 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran; isopropyl alcohol / 75 °C

With 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; diethyl ether; isopropyl alcohol; 2: |Stetter 1,4-Dicarbonyl Synthesis;
DOI:10.1021/ol402017x