ethyl-9-iodononate

Base Information

• Chemical Name: ethyl-9-iodononate
• CAS No.: 57267-52-4
• Molecular Formula: C₁₁H₂₁IO₂
• Molecular Weight: 312.191
• Mol file: 57267-52-4.mol

Synonyms:Ethyl9-iodononanoate

Chemical Property of ethyl-9-iodononate

Chemical Property:

• Vapor Pressure: 0.00146mmHg at 25°C
• Boiling Point: 296.2°C at 760 mmHg
• Flash Point: 132.9°C
• PSA: 26.30000
• Density: 1.343g/cm³
• LogP: 3.71520

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl-9-iodononate

There total 6 articles about ethyl-9-iodononate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-(Toluene-4-sulfonyloxy)-nonanoic acid ethyl ester (189025-36-3) → ethyl 9-iodononanoate (57267-52-4)

Guidance literature:

With lithium iodide; In acetone; for 14h; Heating;

DOI:10.1271/bbb.61.551

Reference yield:

oleic acid ethyl ester (111-62-6) → ethyl 9-iodononanoate (57267-52-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 89 percent / O₃ / methanol / -20 °C

2: NaBH₄ / ethanol

3: pyridine / 0 °C

4: 6.2 g / LiI / acetone / 14 h / Heating

With pyridine; sodium tetrahydroborate; ozone; lithium iodide; In methanol; ethanol; acetone;

DOI:10.1271/bbb.61.551

Reference yield:

ethyl 9-oxononanoate (3433-16-7) → ethyl 9-iodononanoate (57267-52-4)

Guidance literature:

Multi-step reaction with 3 steps

1: NaBH₄ / ethanol

2: pyridine / 0 °C

3: 6.2 g / LiI / acetone / 14 h / Heating

With pyridine; sodium tetrahydroborate; lithium iodide; In ethanol; acetone;

DOI:10.1271/bbb.61.551

upstream raw materials:

9-(Toluene-4-sulfonyloxy)-nonanoic acid ethyl ester

ethyl iodide

oleic acid ethyl ester

ethyl 9-oxononanoate

Refernces

• 1、 Nakajima,Okamura,Takeda,Sugawa,Tateishi,Iwasa,Baba. "Synthesis of 13-oxo-(Z)-9-octadecenoic acid and 15-oxo-(Z)-11-icosenoic acid, arrestants of Oryzaephilus surinamensis L.". . p. 551 - 552. Retrieved 2007/10/03.