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Technology Process of (C2H5)3NCH2Cl(1+)*[Co(NC5H3(CONCH2C6H4O(CH2)5)2)(NC5H3(CONCH2C6H4O(CH2)4CHCH2)2)](1-)=C71H89ClCoN7O8

(C2H5)3NCH2Cl(1+)*[Co(NC5H3(CONCH2C6H4O(CH2)5)2)(NC5H3(CONCH2C6H4O(CH2)4CHCH2)2)](1-)=C71H89ClCoN7O8

Base Information
  • Chemical Name:(C2H5)3NCH2Cl(1+)*[Co(NC5H3(CONCH2C6H4O(CH2)5)2)(NC5H3(CONCH2C6H4O(CH2)4CHCH2)2)](1-)=C71H89ClCoN7O8
  • CAS No.:1134518-50-5
  • Molecular Formula:C7H17ClN*C64H72CoN6O8
  • Molecular Weight:1262.98
  • Hs Code.:
(C<sub>2</sub>H<sub>5</sub>)3NCH<sub>2</sub>Cl<sup>(1+)</sup>*[Co(NC<sub>5</sub>H<sub>3</sub>(CONCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)5)2)(NC<sub>5</sub>H<sub>3</sub>(CONCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)4CHCH<sub>2</sub>)2)]<sup>(1-)</sup>=C<sub>71</sub>H<sub>89</sub>ClCoN<sub>7</sub>O<sub>8</sub>

Synonyms:(C2H5)3NCH2Cl(1+)*[Co(NC5H3(CONCH2C6H4O(CH2)5)2)(NC5H3(CONCH2C6H4O(CH2)4CHCH2)2)](1-)=C71H89ClCoN7O8

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Chemical Property of (C2H5)3NCH2Cl(1+)*[Co(NC5H3(CONCH2C6H4O(CH2)5)2)(NC5H3(CONCH2C6H4O(CH2)4CHCH2)2)](1-)=C71H89ClCoN7O8
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Technology Process of (C2H5)3NCH2Cl(1+)*[Co(NC5H3(CONCH2C6H4O(CH2)5)2)(NC5H3(CONCH2C6H4O(CH2)4CHCH2)2)](1-)=C71H89ClCoN7O8

There total 1 articles about (C2H5)3NCH2Cl(1+)*[Co(NC5H3(CONCH2C6H4O(CH2)5)2)(NC5H3(CONCH2C6H4O(CH2)4CHCH2)2)](1-)=C71H89ClCoN7O8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

dichloromethane
75-09-2

dichloromethane

cobalt(II) diacetate tetrahydrate
6147-53-1

cobalt(II) diacetate tetrahydrate

triethylamine
121-44-8

triethylamine

NC<sub>5</sub>H<sub>3</sub>(CONHCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OCH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>)2
769935-87-7

NC5H3(CONHCH2C6H4OCH2CH2CH2CH2CH2)2

N,N'-bis[4-(hex-5-enyloxy)benzyl]-2,6-pyridinedicarboxamide
769935-77-5

N,N'-bis[4-(hex-5-enyloxy)benzyl]-2,6-pyridinedicarboxamide

(C<sub>2</sub>H<sub>5</sub>)3NCH<sub>2</sub>Cl<sup>(1+)</sup>*[Co(NC<sub>5</sub>H<sub>3</sub>(CONCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)5)2)(NC<sub>5</sub>H<sub>3</sub>(CONCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)4CHCH<sub>2</sub>)2)]<sup>(1-)</sup>=C<sub>71</sub>H<sub>89</sub>ClCoN<sub>7</sub>O<sub>8</sub>
1134518-50-5

(C2H5)3NCH2Cl(1+)*[Co(NC5H3(CONCH2C6H4O(CH2)5)2)(NC5H3(CONCH2C6H4O(CH2)4CHCH2)2)](1-)=C71H89ClCoN7O8

Guidance literature:
With air; sodium ethanolate; In ethanol; a suspn. of ligands, (C2H5)4N(O2CCH3) and Co salt in EtOH refluxed underN2, a soln. of NaOC2H5 in EtOH added, exposed to air for ca 5 min, refl uxed for 25 min; evapd. (vac.), chromd. (silica gel, acetone/(C2H5)3N/CH2Cl2), obtained as an oil;
upstream raw materials:

dichloromethane

cobalt(II) diacetate tetrahydrate

triethylamine

NC5H3(CONHCH2C6H4OCH2CH2CH2CH2CH2)2

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