Technology Process of C31H27NO7
There total 4 articles about C31H27NO7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C30H25NO7;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 0 ℃;
for 0.5h;
methyl iodide;
In
tetrahydrofuran; mineral oil;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C
2.1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / toluene / 20.5 h / 100 °C / Inert atmosphere; Schlenk technique
3.1: mineral oil; tetrahydrofuran / 0.5 h / 0 °C
3.2: 12 h / 0 - 20 °C
With
palladium 10% on activated carbon; hydrogen; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
In
tetrahydrofuran; methanol; toluene; mineral oil;
DOI:10.1021/ja504624q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 °C
1.2: 3 h / 0 - 20 °C
2.1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C
3.1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / toluene / 20.5 h / 100 °C / Inert atmosphere; Schlenk technique
4.1: mineral oil; tetrahydrofuran / 0.5 h / 0 °C
4.2: 12 h / 0 - 20 °C
With
palladium 10% on activated carbon; hydrogen; palladium diacetate; sodium hydride; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
In
tetrahydrofuran; methanol; toluene; mineral oil;
DOI:10.1021/ja504624q
