O-((2,2-difluoro-3-phenethylcyclopropyl)methyl) S-methyl carbonodithioate

Base Information

Chemical Name:O-((2,2-difluoro-3-phenethylcyclopropyl)methyl) S-methyl carbonodithioate
CAS No.:1607805-29-7
Molecular Formula:C₁₄H₁₆F₂OS₂
Molecular Weight:302.409
Hs Code.:

Synonyms:O-((2,2-difluoro-3-phenethylcyclopropyl)methyl) S-methyl carbonodithioate

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Chemical Property of O-((2,2-difluoro-3-phenethylcyclopropyl)methyl) S-methyl carbonodithioate

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Technology Process of O-((2,2-difluoro-3-phenethylcyclopropyl)methyl) S-methyl carbonodithioate

There total 3 articles about O-((2,2-difluoro-3-phenethylcyclopropyl)methyl) S-methyl carbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1607805-34-4
C₁₂H₁₄F₂O

: 74-88-4
methyl iodide

: 1607805-29-7
O-((2,2-difluoro-3-phenethylcyclopropyl)methyl) S-methyl carbonodithioate

Guidance literature:: carbon disulfide; C₁₂H₁₄F₂O; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; hexane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol500803r

Reference yield:

: 126435-89-0
(E)-5-phenyl-2-penten-1-ol acetate

: 1607805-29-7
O-((2,2-difluoro-3-phenethylcyclopropyl)methyl) S-methyl carbonodithioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: diethylene glycol dimethyl ether / 0.5 h / 20 - 180 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 12 h / 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere

3.2: 0.5 h / 20 °C / Inert atmosphere

With n-butyllithium; potassium carbonate; In tetrahydrofuran; methanol; hexane; diethylene glycol dimethyl ether;
DOI:10.1021/ol500803r

Reference yield:

: C₁₄H₁₆F₂O₂

: 1607805-29-7
O-((2,2-difluoro-3-phenethylcyclopropyl)methyl) S-methyl carbonodithioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / methanol / 12 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

With n-butyllithium; potassium carbonate; In tetrahydrofuran; methanol; hexane;
DOI:10.1021/ol500803r