methyl 5-[[4-(2-aminoethyl)-phenyl]sulfonyl]-2-hydroxybenzoate hydrochloride

Base Information

Chemical Name:methyl 5-[[4-(2-aminoethyl)-phenyl]sulfonyl]-2-hydroxybenzoate hydrochloride
CAS No.:699016-47-2
Molecular Formula:C₁₆H₁₇NO₅S*ClH
Molecular Weight:371.842
Hs Code.:

Synonyms:methyl 5-[[4-(2-aminoethyl)-phenyl]sulfonyl]-2-hydroxybenzoate hydrochloride

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Chemical Property of methyl 5-[[4-(2-aminoethyl)-phenyl]sulfonyl]-2-hydroxybenzoate hydrochloride

Chemical Property:

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Technology Process of methyl 5-[[4-(2-aminoethyl)-phenyl]sulfonyl]-2-hydroxybenzoate hydrochloride

There total 1 articles about methyl 5-[[4-(2-aminoethyl)-phenyl]sulfonyl]-2-hydroxybenzoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23069-99-0
N-(2-phenylethyl)formamide

: 60638-81-5
5-chlorosulfonyl-2-hydroxy-benzoicacid methylester

: 699016-47-2
methyl 5-[[4-(2-aminoethyl)-phenyl]sulfonyl]-2-hydroxybenzoate hydrochloride

Guidance literature:: N-(2-phenylethyl)formamide; 5-chlorosulfonyl-2-hydroxy-benzoicacid methylester; With aluminum (III) chloride; In nitrobenzene; at 100 ℃; for 4h;

With hydrogenchloride; In water; ethyl acetate; nitrobenzene; at 0 ℃; for 0.333333h;

With hydrogenchloride; In methanol; at 40 ℃; for 2.5h;

Reference yield:

: 699016-47-2
methyl 5-[[4-(2-aminoethyl)-phenyl]sulfonyl]-2-hydroxybenzoate hydrochloride

: 24424-99-5
di-tert-butyl dicarbonate

: methyl 5-[[4-[2-[(tert-butoxycarbonyl)amino]ethyl]phenyl]sulfonyl]-2-hydroxybenzoate

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 1.5h; pH=8;

Reference yield:

: 699016-47-2
methyl 5-[[4-(2-aminoethyl)-phenyl]sulfonyl]-2-hydroxybenzoate hydrochloride

: 100-52-7
benzaldehyde

: 699016-53-0
methyl 5-[[4-[2-(benzylamino)ethyl]phenyl]sulfonyl]-2-hydroxybenzoate

Guidance literature:: methyl 5-[[4-(2-aminoethyl)-phenyl]sulfonyl]-2-hydroxybenzoate hydrochloride; With potassium carbonate; In methanol; at 20 ℃; for 1.5h;

benzaldehyde; In tetrahydrofuran; at 50 ℃; for 2h;

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 20 ℃; for 2h;