[3-(4-anthracen-9-yl-3,5-bis-hexyloxy-benzyloxy)-5-(3,5-bis-hexyloxy-benzyloxy)-phenyl]-methanol

Base Information

Chemical Name:[3-(4-anthracen-9-yl-3,5-bis-hexyloxy-benzyloxy)-5-(3,5-bis-hexyloxy-benzyloxy)-phenyl]-methanol
CAS No.:848474-51-1
Molecular Formula:C₅₉H₇₆O₇
Molecular Weight:897.248
Hs Code.:

Synonyms:[3-(4-anthracen-9-yl-3,5-bis-hexyloxy-benzyloxy)-5-(3,5-bis-hexyloxy-benzyloxy)-phenyl]-methanol

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Chemical Property of [3-(4-anthracen-9-yl-3,5-bis-hexyloxy-benzyloxy)-5-(3,5-bis-hexyloxy-benzyloxy)-phenyl]-methanol

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Technology Process of [3-(4-anthracen-9-yl-3,5-bis-hexyloxy-benzyloxy)-5-(3,5-bis-hexyloxy-benzyloxy)-phenyl]-methanol

There total 12 articles about [3-(4-anthracen-9-yl-3,5-bis-hexyloxy-benzyloxy)-5-(3,5-bis-hexyloxy-benzyloxy)-phenyl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 848474-41-9
3-(3,5-bis-hexyloxy-benzyloxy)-5-hydroxymethyl-phenol

: 848474-37-3
9-(4-bromomethyl-2,6-bis-hexyloxy-phenyl)-anthracene

: 848474-51-1
[3-(4-anthracen-9-yl-3,5-bis-hexyloxy-benzyloxy)-5-(3,5-bis-hexyloxy-benzyloxy)-phenyl]-methanol

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; for 12h; Heating;
DOI:10.1021/ja043356+

Reference yield:

: 29654-55-5
5-(hydroxymethyl)benzene-1,3-diol

: 848474-51-1
[3-(4-anthracen-9-yl-3,5-bis-hexyloxy-benzyloxy)-5-(3,5-bis-hexyloxy-benzyloxy)-phenyl]-methanol

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

2: 89 percent / CBr₄; Ph₃P

3: 80 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

4: 84 percent / p-TSA / ethanol; CH₂Cl₂ / 20 °C

5: 89 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

With 18-crown-6 ether; carbon tetrabromide; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In ethanol; dichloromethane; acetone;
DOI:10.1021/ja043356+

Reference yield:

: 100622-34-2
anthracene-9-boronic acid

: 848474-51-1
[3-(4-anthracen-9-yl-3,5-bis-hexyloxy-benzyloxy)-5-(3,5-bis-hexyloxy-benzyloxy)-phenyl]-methanol

Guidance literature:: Multi-step reaction with 6 steps

1: K₃PO₄; Pd(PPh₃)4 / 1,2-dimethoxy-ethane / 48 h / Heating

2: p-TSA / ethanol; CH₂Cl₂ / 20 °C

3: 15 percent / LiAlH₄ / tetrahydrofuran / 1 h / 20 °C

4: 69 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

5: 90 percent / CBr₄; Ph₃P

6: 89 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

With potassium phosphate; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 18-crown-6 ether; carbon tetrabromide; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; dichloromethane; acetone;
DOI:10.1021/ja043356+