9-{4-[3-(3,5-bis-hexyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-2,6-bis-hexyloxy-phenyl}-anthracene

Base Information

Chemical Name:9-{4-[3-(3,5-bis-hexyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-2,6-bis-hexyloxy-phenyl}-anthracene
CAS No.:848474-46-4
Molecular Formula:C₅₉H₇₅BrO₆
Molecular Weight:960.145
Hs Code.:

Synonyms:9-{4-[3-(3,5-bis-hexyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-2,6-bis-hexyloxy-phenyl}-anthracene

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Chemical Property of 9-{4-[3-(3,5-bis-hexyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-2,6-bis-hexyloxy-phenyl}-anthracene

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Technology Process of 9-{4-[3-(3,5-bis-hexyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-2,6-bis-hexyloxy-phenyl}-anthracene

There total 14 articles about 9-{4-[3-(3,5-bis-hexyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-2,6-bis-hexyloxy-phenyl}-anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 848474-51-1
[3-(4-anthracen-9-yl-3,5-bis-hexyloxy-benzyloxy)-5-(3,5-bis-hexyloxy-benzyloxy)-phenyl]-methanol

: 848474-46-4
9-{4-[3-(3,5-bis-hexyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-2,6-bis-hexyloxy-phenyl}-anthracene

Guidance literature:: With carbon tetrabromide; triphenylphosphine;
DOI:10.1021/ja043356+

Reference yield:

: 29654-55-5
5-(hydroxymethyl)benzene-1,3-diol

: 848474-46-4
9-{4-[3-(3,5-bis-hexyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-2,6-bis-hexyloxy-phenyl}-anthracene

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

2: 89 percent / CBr₄; Ph₃P

3: 80 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

4: 84 percent / p-TSA / ethanol; CH₂Cl₂ / 20 °C

5: 89 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

6: 74 percent / CBr₄; Ph₃P

With 18-crown-6 ether; carbon tetrabromide; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In ethanol; dichloromethane; acetone;
DOI:10.1021/ja043356+

Reference yield:

: 100622-34-2
anthracene-9-boronic acid

: 848474-46-4
9-{4-[3-(3,5-bis-hexyloxy-benzyloxy)-5-bromomethyl-phenoxymethyl]-2,6-bis-hexyloxy-phenyl}-anthracene

Guidance literature:: Multi-step reaction with 7 steps

1: K₃PO₄; Pd(PPh₃)4 / 1,2-dimethoxy-ethane / 48 h / Heating

2: p-TSA / ethanol; CH₂Cl₂ / 20 °C

3: 15 percent / LiAlH₄ / tetrahydrofuran / 1 h / 20 °C

4: 69 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

5: 90 percent / CBr₄; Ph₃P

6: 89 percent / K₂CO₃; 18-crown-6 / acetone / 12 h / Heating

7: 74 percent / CBr₄; Ph₃P

With potassium phosphate; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 18-crown-6 ether; carbon tetrabromide; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; dichloromethane; acetone;
DOI:10.1021/ja043356+