3,5-dibenzyloxy-4-(2,6-dibenzyloxybenzoyl)benzoic acid 1,1-dimethylethyl ester

Base Information

Chemical Name:3,5-dibenzyloxy-4-(2,6-dibenzyloxybenzoyl)benzoic acid 1,1-dimethylethyl ester
CAS No.:167830-85-5
Molecular Formula:C₄₆H₄₂O₇
Molecular Weight:706.835
Hs Code.:

Synonyms:3,5-dibenzyloxy-4-(2,6-dibenzyloxybenzoyl)benzoic acid 1,1-dimethylethyl ester

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Chemical Property of 3,5-dibenzyloxy-4-(2,6-dibenzyloxybenzoyl)benzoic acid 1,1-dimethylethyl ester

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Technology Process of 3,5-dibenzyloxy-4-(2,6-dibenzyloxybenzoyl)benzoic acid 1,1-dimethylethyl ester

There total 5 articles about 3,5-dibenzyloxy-4-(2,6-dibenzyloxybenzoyl)benzoic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 167830-84-4
3,5-dibenzyloxy-4-(2,6-dibenzyloxybenzylhydroxy)benzoic acid 1,1-dimethylethyl ester

: 167830-85-5
3,5-dibenzyloxy-4-(2,6-dibenzyloxybenzoyl)benzoic acid 1,1-dimethylethyl ester

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In acetone; at 20 ℃; for 0.333333h;
DOI:10.1021/jm020018f

Reference yield:

: 303-07-1
2,6-Dihydroxybenzoic acid

: 167830-85-5
3,5-dibenzyloxy-4-(2,6-dibenzyloxybenzoyl)benzoic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: K₂CO₃ / dimethylformamide / 2 h / 80 °C

1.2: 94 percent / LiAlH₄ / tetrahydrofuran / 20 h / 20 °C

2.1: 34 percent / PDC / CH₂Cl₂ / 72 h / 20 °C

3.1: n-BuLi / tetrahydrofuran; cyclohexane / 0.33 h / -78 °C

3.2: 45 percent / tetrahydrofuran; cyclohexane / 0.5 h / -78 °C

4.1: 87 percent / CrO₃; aq. H₂SO₄ / acetone / 0.33 h / 20 °C

With chromium(VI) oxide; dipyridinium dichromate; n-butyllithium; sulfuric acid; potassium carbonate; In tetrahydrofuran; dichloromethane; cyclohexane; N,N-dimethyl-formamide; acetone; 4.1: Jones oxidation;
DOI:10.1021/jm020018f

Reference yield:

: 25983-53-3
3-((3-(benzyloxy)-2-formylphenoxy)methyl)benzene

: 167830-85-5
3,5-dibenzyloxy-4-(2,6-dibenzyloxybenzoyl)benzoic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; cyclohexane / 0.33 h / -78 °C

1.2: 45 percent / tetrahydrofuran; cyclohexane / 0.5 h / -78 °C

2.1: 87 percent / CrO₃; aq. H₂SO₄ / acetone / 0.33 h / 20 °C

With chromium(VI) oxide; n-butyllithium; sulfuric acid; In tetrahydrofuran; cyclohexane; acetone; 2.1: Jones oxidation;
DOI:10.1021/jm020018f