1,2-dihydro-2-phenyl-1,2-oxaborine

Base Information

Chemical Name:1,2-dihydro-2-phenyl-1,2-oxaborine
CAS No.:935475-67-5
Molecular Formula:C₁₀H₉BO
Molecular Weight:155.992
Hs Code.:

Synonyms:1,2-dihydro-2-phenyl-1,2-oxaborine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-dihydro-2-phenyl-1,2-oxaborine

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Technology Process of 1,2-dihydro-2-phenyl-1,2-oxaborine

There total 1 articles about 1,2-dihydro-2-phenyl-1,2-oxaborine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: (2,3-dihydro-1,2-oxaborol-3-yl)potassium

: 75-09-2
dichloromethane

: 935475-67-5
1,2-dihydro-2-phenyl-1,2-oxaborine

Guidance literature:: With KN(SiMe₃)2; In tetrahydrofuran; dichloromethane; THF was slowly added with stirring to mixt. of KN(SiMe3)2 and B compd. at -78°C; CH2Cl2 was slowly added at -78°C; mixt. was stirred at -78°C for 2 h; slowly warmed to 25°C for 10 h; solvent removed (vac.); extd. (pentane); solvent removed (vac.); distd. (32°C/0.01 Torr); elem. anal.;
DOI:10.1021/om070113s