[Au2(benzoato)2(μ-2-C6H4PEt2)2]

Base Information

Chemical Name:[Au2(benzoato)2(μ-2-C6H4PEt2)2]
CAS No.:183597-79-7
Molecular Formula:C₃₄H₃₈Au₂O₄P₂
Molecular Weight:966.554
Hs Code.:

Synonyms:[Au2(benzoato)2(μ-2-C6H4PEt2)2]

Suppliers and Price of [Au2(benzoato)2(μ-2-C6H4PEt2)2]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Au2(benzoato)2(μ-2-C6H4PEt2)2]

Chemical Property:

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Technology Process of [Au2(benzoato)2(μ-2-C6H4PEt2)2]

There total 2 articles about [Au2(benzoato)2(μ-2-C6H4PEt2)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99177-45-4
1-(diethylphosphino)-2-bromobenzene

: 183597-79-7
[Au2(benzoato)2(μ-2-C6H4PEt2)2]

Guidance literature:: Multi-step reaction with 2 steps

2: dichloromethane

In dichloromethane;
DOI:10.1021/ja961511h

Reference yield:

: bis(μ-(2-diethylphosphino)phenyl)digold(I)

: 94-36-0
dibenzoyl peroxide

: 183597-79-7
[Au2(benzoato)2(μ-2-C6H4PEt2)2]

Guidance literature:: In dichloromethane; reaction in the dark, room temp. (48 h), removal of the solvent, stirring with ether (2 h); evapn. to dryness, dissolution (CH2Cl2), cooling, filtration; elem. anal.;
DOI:10.1021/ja961511h

Reference yield: 80.0%

: 110-54-3
hexane

: 183597-79-7
[Au2(benzoato)2(μ-2-C6H4PEt2)2]

: 344-04-7
bromopentafluorobenzene

: [Au2(pentafluorophenyl)2(μ-2-C6H4PEt2)2]*0.5(hexane)

Guidance literature:: With n-C₄H₉Li; In diethyl ether; hexane; toluene; (N2); C6F5Br/ether cooled in dry ice and treated dropwise with BuLi/hexane, stirred at dry ice temp. for 1 h, treated over 30 min with Au complex/toluene at -70°C, stirred for 30 min, stirred for 3 h at room temp.; filtered (Celite) in air, solvent removed (vac.), toluene soln. chromd. (Al2O3, toluene/hexane), solvent stripped, residue recrystd. (toluene/hexane); elem. anal.;
DOI:10.1021/om000773w