5a-carba-α-D-mannopyranose-6-phosphate

Base Information

Chemical Name:5a-carba-α-D-mannopyranose-6-phosphate
CAS No.:1313195-32-2
Molecular Formula:C₇H₁₅O₈P
Molecular Weight:258.165
Hs Code.:

Synonyms:5a-carba-α-D-mannopyranose-6-phosphate

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Chemical Property of 5a-carba-α-D-mannopyranose-6-phosphate

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Technology Process of 5a-carba-α-D-mannopyranose-6-phosphate

There total 10 articles about 5a-carba-α-D-mannopyranose-6-phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 135820-00-7
5a-carba-α-D-mannopyranose

: 1313195-32-2
5a-carba-α-D-mannopyranose-6-phosphate

Guidance literature:: With pyruvate kinase; phosphoenolpyruvic acid; yeast hexokinase; ammonium bicarbonate; ATP; magnesium chloride; In water; at 30 ℃; for 18h; pH=8.3; aq. buffer; Enzymatic reaction;
DOI:10.1016/j.carres.2011.04.011

Reference yield:

: 1151903-44-4
(1S,2R,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-(benzyloxymethyl)-cyclohexanol

: 1313195-32-2
5a-carba-α-D-mannopyranose-6-phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium(II) hydroxide / water; isopropyl alcohol / 48 h

2: pyruvate kinase; yeast hexokinase; phosphoenolpyruvic acid; ammonium bicarbonate; ATP; magnesium chloride / water / 18 h / 30 °C / pH 8.3 / aq. buffer; Enzymatic reaction

With pyruvate kinase; phosphoenolpyruvic acid; yeast hexokinase; hydrogen; palladium(II) hydroxide; ammonium bicarbonate; ATP; magnesium chloride; In water; isopropyl alcohol;
DOI:10.1016/j.carres.2011.04.011

Reference yield:

: 1313195-33-3
(1S,4S,5R)-4-O-benzyl-5-benzyloxymethyl-1-O-(tert-butyldimethylsilyl)cyclohex-2-en-1,4-diol

: 1313195-32-2
5a-carba-α-D-mannopyranose-6-phosphate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium osmate(VI); 4-methylmorpholine N-oxide / water; acetone / 16 h / 20 °C

2.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 20 °C

4.1: hydrogen; palladium(II) hydroxide / water; isopropyl alcohol / 48 h

5.1: pyruvate kinase; yeast hexokinase; phosphoenolpyruvic acid; ammonium bicarbonate; ATP; magnesium chloride / water / 18 h / 30 °C / pH 8.3 / aq. buffer; Enzymatic reaction

With potassium osmate(VI); pyruvate kinase; phosphoenolpyruvic acid; yeast hexokinase; tetrabutyl ammonium fluoride; hydrogen; palladium(II) hydroxide; tetra-(n-butyl)ammonium iodide; sodium hydride; ammonium bicarbonate; 4-methylmorpholine N-oxide; ATP; magnesium chloride; In tetrahydrofuran; water; isopropyl alcohol; acetone;
DOI:10.1016/j.carres.2011.04.011