Technology Process of C14H21NO6S2
There total 5 articles about C14H21NO6S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at -6 - 20 ℃;
Inert atmosphere;
Cooling with acetone-dry ice;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: diethyl ether / 8 - 20 °C / Inert atmosphere; Cooling with ice
2: N,N-dimethyl-formamide / 18 - 95 °C / Inert atmosphere
3: methanol; sodium tetrahydroborate / tetrahydrofuran / -4 - 20 °C / Cooling with acetone-dry ice; Inert atmosphere
4: triethylamine / dichloromethane / -6 - 20 °C / Inert atmosphere; Cooling with acetone-dry ice
With
methanol; sodium tetrahydroborate; triethylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 18 - 95 °C / Inert atmosphere
2: methanol; sodium tetrahydroborate / tetrahydrofuran / -4 - 20 °C / Cooling with acetone-dry ice; Inert atmosphere
3: triethylamine / dichloromethane / -6 - 20 °C / Inert atmosphere; Cooling with acetone-dry ice
With
methanol; sodium tetrahydroborate; triethylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;