5-CHLORO-2,4-DINITROTOLUENE

Base Information

• Chemical Name: 5-CHLORO-2,4-DINITROTOLUENE
• CAS No.: 51676-74-5
• Molecular Formula: C7H5ClN2O4
• Molecular Weight: 216.581
• Hs Code.: 29049090
• Mol file: 51676-74-5.mol

Synonyms:Toluene,5-chloro-2,4-dinitro- (6CI,7CI);1-Chloro-3-methyl-4,6-dinitrobenzene;1-Chloro-4,6-dinitro-3-methylbenzene;1-Chloro-5-methyl-2,4-dinitrobenzene;3-Chloro-4,6-dinitrotoluene;5-Chloro-2,4-dinitrotoluene;NSC 77049;

Chemical Property of 5-CHLORO-2,4-DINITROTOLUENE

Chemical Property:

• Vapor Pressure: 0.000255mmHg at 25°C
• Melting Point: 87-91 °C(lit.)
• Refractive Index: 1.61
• Boiling Point: 334 °C at 760 mmHg
• Flash Point: 155.8 °C
• PSA: 91.64000
• Density: 1.532 g/cm³
• LogP: 3.51120

Purity/Quality:

99% ^*data from raw suppliers

5-Chloro-2,4-dinitrotoluene ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 43
• Safety Statements: 36/37

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: 5-Chloro-2,4-dinitrotoluene (5CDNT) may be used to synthesize 5-methyl-6-nitrobenzofuroxan.

Technology Process of 5-CHLORO-2,4-DINITROTOLUENE

There total 7 articles about 5-CHLORO-2,4-DINITROTOLUENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

5-amino-2,4-dinitrotoluene (5267-27-6) → 1-chloro-5-methyl-2,4-dinitrobenzene (51676-74-5)

Guidance literature:

With tert.-butylnitrite; copper dichloride; In acetonitrile; at 65 ℃; for 2h;

DOI:10.1016/0040-4020(89)80127-9

Reference yield: 60.0%

1-chloro-3-methylbenzene (108-41-8) → 1-chloro-5-methyl-2,4-dinitrobenzene (51676-74-5)

Guidance literature:

With sulfuric acid; nitric acid; at 0 - 35 ℃; for 0.5h;

Reference yield:

2-chloro-1-isopropyl-4-methyl-benzene (4395-80-6) → 1-chloro-5-methyl-2,4-dinitrobenzene (51676-74-5) + 2-chloro-1-isopropyl-4-methyl-3,5-dinitro-benzene (854821-48-0)

Guidance literature:

With sulfuric acid; nitric acid;

upstream raw materials:

1-chloro-3-methylbenzene

2-chloro-1-isopropyl-4-methyl-benzene

5-amino-2,4-dinitrotoluene

2,4,5-trinitrotoluene

Downstream raw materials:

(5-methyl-2,4-dinitro-phenyl)-malonic acid diethyl ester

5-methyl-6-nitro-2-p-tolyl-2H-benzotriazole

1-(5-methyl-2,4-dinitro-phenyl)-piperidine

2-(5-methyl-2,4-dinitro-phenyl)-acetoacetic acid ethyl ester