2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-D-glucopyranose O-benzyl oxime ether

Base Information

Chemical Name:2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-D-glucopyranose O-benzyl oxime ether
CAS No.:144989-59-3
Molecular Formula:C₂₇H₃₂N₂O₁₀
Molecular Weight:544.558
Hs Code.:

Synonyms:2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-D-glucopyranose O-benzyl oxime ether

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Chemical Property of 2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-D-glucopyranose O-benzyl oxime ether

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Technology Process of 2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-D-glucopyranose O-benzyl oxime ether

There total 10 articles about 2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-D-glucopyranose O-benzyl oxime ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 140183-55-7
2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-5-imidazol-1-ylthiocarbonyloxy-D-glucononitrile

: 144989-59-3
2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-D-glucopyranose O-benzyl oxime ether

Guidance literature:: With pyridine; In dichloromethane;
DOI:10.1016/S0040-4039(00)77717-3

Reference yield: 88.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 99194-76-0,140183-53-5
2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-D-glucopyranose

: 144989-59-3
2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-D-glucopyranose O-benzyl oxime ether

Guidance literature:: With pyridine; In dichloromethane; for 168h; Ambient temperature;

Reference yield:

: 35946-66-8
2-(acetoxymethyl)-5-{[(benzyloxy)carbonyl]amino}tetrahydropyran-3,4,6-triyl triacetate

: 144989-59-3
2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-D-glucopyranose O-benzyl oxime ether

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / (NH₄)2CO₃ / methanol; tetrahydrofuran

2: 74 percent / NH₂OH*HCl, pyridine / methanol

3: 58 percent / CH₂Cl₂

4: 88 percent / pyridine / CH₂Cl₂

With pyridine; hydroxylamine hydrochloride; ammonium carbonate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/S0040-4039(00)77717-3