10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-N,N-diphenyl-10H-phenothiazin-2-amine

Base Information

• Chemical Name: 10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-N,N-diphenyl-10H-phenothiazin-2-amine
• CAS No.: 1401710-54-0
• Molecular Formula: C₃₆H₂₈N₆OS
• Molecular Weight: 592.724
• Mol file: 1401710-54-0.mol

Synonyms:10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-N,N-diphenyl-10H-phenothiazin-2-amine

Chemical Property of 10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-N,N-diphenyl-10H-phenothiazin-2-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-N,N-diphenyl-10H-phenothiazin-2-amine

There total 1 articles about 10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-N,N-diphenyl-10H-phenothiazin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine (742105-63-1) + diphenylamine (122-39-4) → 10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-N,N-diphenyl-10H-phenothiazin-2-amine (1401710-54-0)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; XPhos; In toluene; at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.07.083

Reference yield: 49.0%

10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-N,N-diphenyl-10H-phenothiazin-2-amine (1401710-54-0) → 1-[2-(diphenylamino)-10H-phenothiazin-10-yl]-4-[2-(4-methoxyphenyl)-2H-tetrazol-5-yl]butan-2-ol (1442371-68-7)

Guidance literature:

10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-N,N-diphenyl-10H-phenothiazin-2-amine; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃; for 24h;

With dihydrogen peroxide; sodium hydroxide; In methanol; water; at 0 - 20 ℃; for 24h;

DOI:10.1016/j.bmc.2013.04.034

upstream raw materials:

2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine

diphenylamine

Downstream raw materials:

1-[2-(diphenylamino)-10H-phenothiazin-10-yl]-4-[2-(4-methoxyphenyl)-2H-tetrazol-5-yl]butan-2-ol