2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine

Base Information

• Chemical Name: 2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine
• CAS No.: 742105-63-1
• Molecular Formula: C₂₄H₁₈ClN₅OS
• Molecular Weight: 459.959

Synonyms:2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine

Chemical Property of 2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine

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Technology Process of 2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine

There total 1 articles about 2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

2-chlorophenothiazine (92-39-7) + 3-(4-methoxyphenyl)-tetrazolo[1,5-a]pyridin-4-ium tetrafluoroborate → 2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine (742105-63-1)

Guidance literature:

With sodium hydride; In tetrahydrofuran; mineral oil; for 48.3333h;

DOI:10.1016/j.bmc.2012.05.065

Reference yield: 86.0%

piperidine (110-89-4) + 2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine (742105-63-1) → 10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-2-(piperidin-1-yl)-10H-phenothiazine (1401710-57-3)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; XPhos; In toluene; at 110 ℃; for 2.5h; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.07.083

Reference yield: 86.0%

acetamide (60-35-5) + 2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine (742105-63-1) → N-(10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazin-2-yl)acetamide (1401710-60-8)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; XPhos; In toluene; at 120 ℃; for 19h; Sealed tube; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.07.083

upstream raw materials:

2-chlorophenothiazine

Downstream raw materials:

6-((2-chloro-10H-phenothiazin-10-yl)methyl)-2-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2H-tetrazolo[5,1-f][1,2]azaborinin-4-ium-5-uide

1-(2-chloro-10H-phenothiazin-10-yl)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)butan-2-ol

4-(2-chloro-10H-phenothiazin-10-yl)-1-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)butane-1,3-diol

2-chloro-10-(2-hydroxy-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)butyl)-10H-phenothiazine 5-oxide

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