1-(Fluoren-9-ylidene)-1-methoxy-1-phenylmethane

Base Information

Chemical Name:1-(Fluoren-9-ylidene)-1-methoxy-1-phenylmethane
CAS No.:27808-13-5
Molecular Formula:C₂₁H₁₆O
Molecular Weight:284.357
Hs Code.:

Synonyms:1-(Fluoren-9-ylidene)-1-methoxy-1-phenylmethane

Suppliers and Price of 1-(Fluoren-9-ylidene)-1-methoxy-1-phenylmethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(Fluoren-9-ylidene)-1-methoxy-1-phenylmethane

Chemical Property:

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Technology Process of 1-(Fluoren-9-ylidene)-1-methoxy-1-phenylmethane

There total 12 articles about 1-(Fluoren-9-ylidene)-1-methoxy-1-phenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 486-25-9,952573-42-1
9-fluorenone

: 132205-80-2,62456-45-5
dimethyl phosphonate

: 27808-13-5
1-(Fluoren-9-ylidene)-1-methoxy-1-phenylmethane

Guidance literature:: dimethyl phosphonate; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

9-fluorenone; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 6h; Further stages.;
DOI:10.1039/b002101f

Reference yield:

: 67-56-1
methanol

: 33735-95-4
9-[bromo-(phenyl)methylene]-9H-fluorene

: 486-25-9,952573-42-1
9-fluorenone

: 27808-13-5
1-(Fluoren-9-ylidene)-1-methoxy-1-phenylmethane

Guidance literature:: With oxygen; sodium methylate; Quantum yield; Mechanism; Irradiation; different wavelength;
DOI:10.1016/S0040-4020(01)88173-4

Reference yield:

: 67-56-1
methanol

: 86457-77-4
(α-Chlorobenzylidene)fluorene

: 486-25-9,952573-42-1
9-fluorenone

: 27808-13-5
1-(Fluoren-9-ylidene)-1-methoxy-1-phenylmethane

: 1836-87-9
9-Benzylidene-9H-fluorene

Guidance literature:: Product distribution; Quantum yield; Ambient temperature; Irradiation; with/without O₂ addition; with/without AcCN solvent;
DOI:10.1021/j100089a027