benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetate

Base Information

Chemical Name:benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetate
CAS No.:1181104-56-2
Molecular Formula:C₂₃H₃₀NO₇P
Molecular Weight:463.467
Hs Code.:

Synonyms:benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetate

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Chemical Property of benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetate

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Technology Process of benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetate

There total 5 articles about benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1181104-51-7
methyl hydrogen [(R,S)-1-(benzyloxycarbonylamino)pent-1-yl]phosphonate

: 30379-58-9
benzyl glycolate

: 1181104-56-2
benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetate

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.tet.2009.05.051

Reference yield:

: 110-62-3
pentanal

: 1181104-56-2
benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetyl chloride / -5 - 20 °C

2.1: sodium hydroxide / methanol; water / 4 h / 80 °C

2.2: pH 1

3.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 20 °C

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; sodium hydroxide; In methanol; water; acetyl chloride; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2009.05.051

Reference yield:

: 621-84-1
O-benzyl carbamate

: 1181104-56-2
benzyl {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetyl chloride / -5 - 20 °C

2.1: sodium hydroxide / methanol; water / 4 h / 80 °C

2.2: pH 1

3.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 20 °C

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; sodium hydroxide; In methanol; water; acetyl chloride; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2009.05.051