4-{3-[(2-fluorobenzyl)oxy]benzoyl}-N-pyridin-3-ylpiperazine-1-carboxamide oxalate

Base Information

Chemical Name:4-{3-[(2-fluorobenzyl)oxy]benzoyl}-N-pyridin-3-ylpiperazine-1-carboxamide oxalate
CAS No.:1008764-29-1
Molecular Formula:C₂H₂O₄*C₂₄H₂₃FN₄O₃
Molecular Weight:524.506
Hs Code.:

Synonyms:4-{3-[(2-fluorobenzyl)oxy]benzoyl}-N-pyridin-3-ylpiperazine-1-carboxamide oxalate

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Chemical Property of 4-{3-[(2-fluorobenzyl)oxy]benzoyl}-N-pyridin-3-ylpiperazine-1-carboxamide oxalate

Chemical Property:

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Technology Process of 4-{3-[(2-fluorobenzyl)oxy]benzoyl}-N-pyridin-3-ylpiperazine-1-carboxamide oxalate

There total 5 articles about 4-{3-[(2-fluorobenzyl)oxy]benzoyl}-N-pyridin-3-ylpiperazine-1-carboxamide oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1008764-28-0
4-{3-[(2-fluorobenzyl)oxy]benzoyl}-N-pyridin-3-ylpiperazine-1-carboxamide

: 144-62-7,97993-78-7
oxalic acid

: 1008764-29-1
4-{3-[(2-fluorobenzyl)oxy]benzoyl}-N-pyridin-3-ylpiperazine-1-carboxamide oxalate

Guidance literature:: In ethanol; at 20 ℃; for 0.5h;

Reference yield:

: 1008763-98-1
4-[3-(benzyloxy)benzoyl]-N-pyridin-3-ylpiperazine-1-carboxamide

: 1008764-29-1
4-{3-[(2-fluorobenzyl)oxy]benzoyl}-N-pyridin-3-ylpiperazine-1-carboxamide oxalate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / ethanol / 5 h

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 20 °C

3: ethanol / 0.5 h / 20 °C

With hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; toluene;

Reference yield:

: piperazine-1-carboxylic acid pyridin-3-ylamide bis-hydrochloride salt

: 1008764-29-1
4-{3-[(2-fluorobenzyl)oxy]benzoyl}-N-pyridin-3-ylpiperazine-1-carboxamide oxalate

Guidance literature:: Multi-step reaction with 4 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 20 °C

2: hydrogen / palladium 10% on activated carbon / ethanol / 5 h

3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 20 °C

4: ethanol / 0.5 h / 20 °C

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene;