5-<(Z)-pentadec-8-enyl>resorcinol dimethyl ether

Base Information

Chemical Name:5-<(Z)-pentadec-8-enyl>resorcinol dimethyl ether
CAS No.:22910-87-8
Molecular Formula:C₂₃H₃₈O₂
Molecular Weight:346.554
Hs Code.:

Synonyms:5-<(Z)-pentadec-8-enyl>resorcinol dimethyl ether

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Chemical Property of 5-<(Z)-pentadec-8-enyl>resorcinol dimethyl ether

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Technology Process of 5-<(Z)-pentadec-8-enyl>resorcinol dimethyl ether

There total 18 articles about 5-<(Z)-pentadec-8-enyl>resorcinol dimethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 52483-34-8
5-(pentadec-8-ynyl)resorcinol dimethyl ether

: 22910-87-8
5-<(Z)-pentadec-8-enyl>resorcinol dimethyl ether

Guidance literature:: With quinoline; Lindlar's catalyst; hydrogen; In cyclohexane; for 4h;
DOI:10.1080/10286020.2011.554828

Reference yield:

: 629-05-0
n-octyne

: 22910-87-8
5-<(Z)-pentadec-8-enyl>resorcinol dimethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, hexamethylphosphoramide / 1.) hexane, 0 deg C, 30 min, 2.) THF, RT, 12 h

2: 87 percent / H₂, quinoline / 5percent Pd/CaCO₃ / cyclohexane / 1 h / 760 Torr

With quinoline; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; hydrogen; Lindlar's catalyst; In cyclohexane;
DOI:10.1021/ja00156a004

Reference yield:

: 21433-45-4
1-octynyllithium

: 22910-87-8
5-<(Z)-pentadec-8-enyl>resorcinol dimethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / 7.5 h / Heating

In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/jo962423i