(2S)-3-methyl-N-[(1E)-phenylmethylidene]-1-[(trimethylsilyl)oxy]-2-butanamine

Base Information

Chemical Name:(2S)-3-methyl-N-[(1E)-phenylmethylidene]-1-[(trimethylsilyl)oxy]-2-butanamine
CAS No.:887330-11-2
Molecular Formula:C₁₅H₂₅NOSi
Molecular Weight:263.455
Hs Code.:

Synonyms:(2S)-3-methyl-N-[(1E)-phenylmethylidene]-1-[(trimethylsilyl)oxy]-2-butanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-3-methyl-N-[(1E)-phenylmethylidene]-1-[(trimethylsilyl)oxy]-2-butanamine

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Technology Process of (2S)-3-methyl-N-[(1E)-phenylmethylidene]-1-[(trimethylsilyl)oxy]-2-butanamine

There total 1 articles about (2S)-3-methyl-N-[(1E)-phenylmethylidene]-1-[(trimethylsilyl)oxy]-2-butanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 75-77-4
chloro-trimethyl-silane

: 84983-97-1
N-benzylidene-L-valinol

: 887330-11-2
(2S)-3-methyl-N-[(1E)-phenylmethylidene]-1-[(trimethylsilyl)oxy]-2-butanamine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 72h;

Reference yield: 86.0%

: 887330-11-2
(2S)-3-methyl-N-[(1E)-phenylmethylidene]-1-[(trimethylsilyl)oxy]-2-butanamine

: 4333-56-6,130561-87-4
cyclopropyl bromide

: (2S)-N-[(S)-cyclopropyl(phenyl)methyl]-3-methyl-1-[(trimethylsilyl)oxy]-2-butanamine

Guidance literature:: cyclopropyl bromide; With tert.-butyl lithium; In diethyl ether; pentane; at -78 - 20 ℃; for 1.16667h;

(2S)-3-methyl-N-[(1E)-phenylmethylidene]-1-[(trimethylsilyl)oxy]-2-butanamine; In diethyl ether; pentane; at -40 ℃; for 1.5h;

With hydrogenchloride; potassium hydroxide; more than 3 stages;

Reference yield: 86.0%

: 887330-11-2
(2S)-3-methyl-N-[(1E)-phenylmethylidene]-1-[(trimethylsilyl)oxy]-2-butanamine

: 4333-56-6,130561-87-4
cyclopropyl bromide

: 844470-77-5
(S)-2-[((S)-1-cyclopropyl-1-phenyl-methyl)-amino]-3-methyl-butan-1-ol

Guidance literature:: cyclopropyl bromide; With tert.-butyl lithium; In diethyl ether; pentane; at -78 - 20 ℃; for 1.16667h;

(2S)-3-methyl-N-[(1E)-phenylmethylidene]-1-[(trimethylsilyl)oxy]-2-butanamine; In diethyl ether; pentane; at -40 ℃; for 1.5h;

With hydrogenchloride; potassium hydroxide; more than 3 stages;