4,4'-bis[N,N'-di(tert-butoxycarbonyl)isoureido]diphenyl thioether

Base Information

• Chemical Name: 4,4'-bis[N,N'-di(tert-butoxycarbonyl)isoureido]diphenyl thioether
• CAS No.: 1073524-86-3
• Molecular Formula: C₃₄H₄₆N₄O₁₀S
• Molecular Weight: 702.826
• Mol file: 1073524-86-3.mol

Synonyms:4,4'-bis[N,N'-di(tert-butoxycarbonyl)isoureido]diphenyl thioether

Chemical Property of 4,4'-bis[N,N'-di(tert-butoxycarbonyl)isoureido]diphenyl thioether

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4,4'-bis[N,N'-di(tert-butoxycarbonyl)isoureido]diphenyl thioether

There total 1 articles about 4,4'-bis[N,N'-di(tert-butoxycarbonyl)isoureido]diphenyl thioether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

4,4'-Thiodiphenol (2664-63-3) + tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate (145013-05-4) → 1,3-di(tert-butoxycarbonyl)-2-[4-(4-hydroxyphenylsulfanyl)phenyl]isourea (1073524-90-9) + 4,4'-bis[N,N'-di(tert-butoxycarbonyl)isoureido]diphenyl thioether (1073524-86-3)

Guidance literature:

With triethylamine; mercury dichloride; In dichloromethane; at 0 - 20 ℃; for 17h;

DOI:10.1016/j.bmc.2008.07.033

Reference yield: 92.0%

4,4'-bis[N,N'-di(tert-butoxycarbonyl)isoureido]diphenyl thioether (1073524-86-3) → 4,4'-diisouronium diphenylthioether dichloride

Guidance literature:

4,4'-bis[N,N'-di(tert-butoxycarbonyl)isoureido]diphenyl thioether; With trifluoroacetic acid; In dichloromethane; for 3h;

With water;

DOI:10.1016/j.bmc.2008.07.033

upstream raw materials:

4,4'-Thiodiphenol

tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate