(Z)-2-[1,3-bis-(2',6'-dimethylphenyl)-2,3-dihydro-1H-1,3,2-diazaphospholyl]-3-diphenylphosphanyl-acrylic acid ethyl ester

Base Information

Chemical Name:(Z)-2-[1,3-bis-(2',6'-dimethylphenyl)-2,3-dihydro-1H-1,3,2-diazaphospholyl]-3-diphenylphosphanyl-acrylic acid ethyl ester
CAS No.:940959-83-1
Molecular Formula:C₃₅H₃₆N₂O₂P₂
Molecular Weight:578.631
Hs Code.:

Synonyms:(Z)-2-[1,3-bis-(2',6'-dimethylphenyl)-2,3-dihydro-1H-1,3,2-diazaphospholyl]-3-diphenylphosphanyl-acrylic acid ethyl ester

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Chemical Property of (Z)-2-[1,3-bis-(2',6'-dimethylphenyl)-2,3-dihydro-1H-1,3,2-diazaphospholyl]-3-diphenylphosphanyl-acrylic acid ethyl ester

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Technology Process of (Z)-2-[1,3-bis-(2',6'-dimethylphenyl)-2,3-dihydro-1H-1,3,2-diazaphospholyl]-3-diphenylphosphanyl-acrylic acid ethyl ester

There total 1 articles about (Z)-2-[1,3-bis-(2',6'-dimethylphenyl)-2,3-dihydro-1H-1,3,2-diazaphospholyl]-3-diphenylphosphanyl-acrylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 905994-36-7
C₂H₂N₂(2,6-dimethylbenzene)PPPh₂

: 623-47-2
propynoic acid ethyl ester

: 940959-83-1
(Z)-2-[1,3-bis-(2',6'-dimethylphenyl)-2,3-dihydro-1H-1,3,2-diazaphospholyl]-3-diphenylphosphanyl-acrylic acid ethyl ester

Guidance literature:: In toluene; at 20 ℃; for 1h;
DOI:10.1002/anie.200604622

Reference yield: 84.0%

: 940959-83-1
(Z)-2-[1,3-bis-(2',6'-dimethylphenyl)-2,3-dihydro-1H-1,3,2-diazaphospholyl]-3-diphenylphosphanyl-acrylic acid ethyl ester

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: [(Z)-2-[1,3-bis(2,6-dimethylphenyl)-2,3-dihydro-1H-1,3,2-diazaphosphol-2-yl]-3-(diphenylphosphanyl)acrylic acid ethyl ester]dichloro palladium(II)

Guidance literature:: In tetrahydrofuran; acetonitrile; (Ar); 1,3,2-diazaphosphol deriv. and (COD)PdCl2 mixed with THF; CH3CN added until dissolution; stored at -20°C until crystn.; filtered; dried in vac.; elem. anal.;
DOI:10.1515/znb-2009-0109