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Technology Process of ((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)(1+)*I(1-)=((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)I

((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)(1+)*I(1-)=((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)I

Base Information
  • Chemical Name:((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)(1+)*I(1-)=((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)I
  • CAS No.:89463-04-7
  • Molecular Formula:C31H29As2CoI*I
  • Molecular Weight:864.217
  • Hs Code.:
((C<sub>5</sub>H<sub>5</sub>)Co((C<sub>6</sub>H<sub>5</sub>)2AsCH<sub>2</sub>CH<sub>2</sub>As(C<sub>6</sub>H<sub>5</sub>)2)I)<sup>(1+)</sup>*I<sup>(1-)</sup>=((C<sub>5</sub>H<sub>5</sub>)Co((C<sub>6</sub>H<sub>5</sub>)2AsCH<sub>2</sub>CH<sub>2</sub>As(C<sub>6</sub>H<sub>5</sub>)2)I)I

Synonyms:((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)(1+)*I(1-)=((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)I

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Chemical Property of ((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)(1+)*I(1-)=((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)I
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Technology Process of ((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)(1+)*I(1-)=((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)I

There total 1 articles about ((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)(1+)*I(1-)=((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

carbonyl(η-5-cyclopentadienyl)diiodocobalt(III)

carbonyl(η-5-cyclopentadienyl)diiodocobalt(III)

1,2-bis(diphenylarsino)ethane
4431-24-7

1,2-bis(diphenylarsino)ethane

((C<sub>5</sub>H<sub>5</sub>)Co((C<sub>6</sub>H<sub>5</sub>)2AsCH<sub>2</sub>CH<sub>2</sub>As(C<sub>6</sub>H<sub>5</sub>)2)I)<sup>(1+)</sup>*I<sup>(1-)</sup>=((C<sub>5</sub>H<sub>5</sub>)Co((C<sub>6</sub>H<sub>5</sub>)2AsCH<sub>2</sub>CH<sub>2</sub>As(C<sub>6</sub>H<sub>5</sub>)2)I)I
89463-04-7

((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)(1+)*I(1-)=((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)I

(C<sub>5</sub>H<sub>5</sub>)CoI<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)2AsCH<sub>2</sub>CH<sub>2</sub>As(C<sub>6</sub>H<sub>5</sub>)2)I<sub>2</sub>Co(C<sub>5</sub>H<sub>5</sub>)

(C5H5)CoI2((C6H5)2AsCH2CH2As(C6H5)2)I2Co(C5H5)

Guidance literature:
In benzene; to soln. CpCoI2(CO) in C6H6 added dropwise soln. dpae in C6H6; after 3 h ppt. filtered, washed with C6H6, Et2O and pentane - (CpCo(dpae)I)I; filtrate concd. - green solid; elem. anal.;

Reference yield: 53.0%

((C<sub>5</sub>H<sub>5</sub>)Co((C<sub>6</sub>H<sub>5</sub>)2AsCH<sub>2</sub>CH<sub>2</sub>As(C<sub>6</sub>H<sub>5</sub>)2)I)<sup>(1+)</sup>*I<sup>(1-)</sup>=((C<sub>5</sub>H<sub>5</sub>)Co((C<sub>6</sub>H<sub>5</sub>)2AsCH<sub>2</sub>CH<sub>2</sub>As(C<sub>6</sub>H<sub>5</sub>)2)I)I
89463-04-7

((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)(1+)*I(1-)=((C5H5)Co((C6H5)2AsCH2CH2As(C6H5)2)I)I

phosphorous acid trimethyl ester
121-45-9

phosphorous acid trimethyl ester

((C<sub>5</sub>H<sub>5</sub>)Co(PO(OCH<sub>3</sub>)2)(P(OCH<sub>3</sub>)3))

((C5H5)Co(PO(OCH3)2)(P(OCH3)3))

1,2-bis(diphenylarsino)ethane
4431-24-7

1,2-bis(diphenylarsino)ethane

Guidance literature:
In dichloromethane; CH2Cl2 soln. (CpCo(dpae)I)I reacted with P(OCH3)3 with stirring for 1 h; solvent removed, solid chromed. on silica with CH2Cl2 and acetone;
upstream raw materials:

1,2-bis(diphenylarsino)ethane

Downstream raw materials:

1,2-bis(diphenylarsino)ethane

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