(S)-2-((tert-butoxycarbonylmethyl)ethylamino)butanoic acid benzyl ester

Base Information

Chemical Name:(S)-2-((tert-butoxycarbonylmethyl)ethylamino)butanoic acid benzyl ester
CAS No.:1259396-68-3
Molecular Formula:C₁₉H₂₉NO₄
Molecular Weight:335.444
Hs Code.:

Synonyms:(S)-2-((tert-butoxycarbonylmethyl)ethylamino)butanoic acid benzyl ester

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Chemical Property of (S)-2-((tert-butoxycarbonylmethyl)ethylamino)butanoic acid benzyl ester

Chemical Property:

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Technology Process of (S)-2-((tert-butoxycarbonylmethyl)ethylamino)butanoic acid benzyl ester

There total 4 articles about (S)-2-((tert-butoxycarbonylmethyl)ethylamino)butanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1259396-54-7
(S)-2-ethylaminobutanoic acid benzyl ester

: 1259396-68-3
(S)-2-((tert-butoxycarbonylmethyl)ethylamino)butanoic acid benzyl ester

Guidance literature:: With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 15h;

Reference yield:

: 100-39-0
benzyl bromide

: 1259396-68-3
(S)-2-((tert-butoxycarbonylmethyl)ethylamino)butanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C

2: hydrogenchloride / ethyl acetate; water / 3 h / 20 °C

3: sodium cyanoborohydride; methanol / 2 h / 20 °C

4: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 15 h / 20 °C

With hydrogenchloride; methanol; sodium cyanoborohydride; potassium carbonate; sodium iodide; In water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 80226-63-7
(S)-2-amino-butyric acid benzyl ester

: 1259396-68-3
(S)-2-((tert-butoxycarbonylmethyl)ethylamino)butanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanoborohydride; methanol / 2 h / 20 °C

2: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 15 h / 20 °C

With methanol; sodium cyanoborohydride; potassium carbonate; sodium iodide; In N,N-dimethyl-formamide;