1-iodo-4-{[1-methoxy-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}benzene

Base Information

Chemical Name:1-iodo-4-{[1-methoxy-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}benzene
CAS No.:1344700-02-2
Molecular Formula:C₁₃H₁₅IN₂O₄
Molecular Weight:390.178
Hs Code.:

Synonyms:1-iodo-4-{[1-methoxy-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}benzene

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Chemical Property of 1-iodo-4-{[1-methoxy-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}benzene

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Technology Process of 1-iodo-4-{[1-methoxy-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}benzene

There total 7 articles about 1-iodo-4-{[1-methoxy-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1344700-01-1
N,N²,O-trimethyl-3-oxoserinamide hydrochloride

: 1711-02-0
4-iodobenzoic acid chloride

: 1344700-02-2
1-iodo-4-{[1-methoxy-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}benzene

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In chloroform; at 20 ℃; for 4h; Cooling with ice;

Reference yield:

: 1032-02-6
diethyl 2-(benzyl(methyl)amino)propanedioate

: 1344700-02-2
1-iodo-4-{[1-methoxy-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}benzene

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 30 h / 20 °C

2: methanol / 114.96 h / 20 °C

3: hydrogenchloride / ethyl acetate / 24 h / 20 °C

4: N-ethyl-N,N-diisopropylamine / chloroform / 4 h / 20 °C / Cooling with ice

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; In methanol; ethanol; chloroform; ethyl acetate;

Reference yield:

: 5417-21-0
dimethyl [benzyl(methyl)amino]propanedioate

: 1344700-02-2
1-iodo-4-{[1-methoxy-3-(methylamino)-1,3-dioxopropan-2-yl](methyl)carbamoyl}benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 26 h / 20 °C

2.1: hydrogen; palladium on carbon / methanol / 3.5 h / 20 °C

2.2: 1.25 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / chloroform / 4 h / 20 °C / Cooling with ice

With palladium on carbon; hydrogen; N-ethyl-N,N-diisopropylamine; In methanol; chloroform;