1-Iodo-3,3-dimethyl-1-butyne

Base Information

Chemical Name:1-Iodo-3,3-dimethyl-1-butyne
CAS No.:23700-63-2
Molecular Formula:C6H9 I
Molecular Weight:208.042
Hs Code.:
DSSTox Substance ID:DTXSID70178366
Nikkaji Number:J756.922J
Wikidata:Q83048749
Mol file:23700-63-2.mol

Synonyms:1-Iodo-3,3-dimethyl-1-butyne;1-iodo-3,3-dimethylbut-1-yne;23700-63-2;1-Iodo-3.3-dimethylbutyne;DTXSID70178366;AT14291

Suppliers and Price of 1-Iodo-3,3-dimethyl-1-butyne

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-Iodo-3,3-dimethyl-1-butyne

Chemical Property:

Vapor Pressure:2.45mmHg at 25°C
Boiling Point:165.5°C at 760 mmHg
Flash Point:57.3°C
Density:1.603g/cm³
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:207.97490
Heavy Atom Count:7
Complexity:105

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C#CI

Technology Process of 1-Iodo-3,3-dimethyl-1-butyne

There total 4 articles about 1-Iodo-3,3-dimethyl-1-butyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 917-92-0
3,3-Dimethylbut-1-yne

: 23700-63-2
1-iodo-3,3-dimethylbut-1-yne

Guidance literature:: 3,3-Dimethylbut-1-yne; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

With iodine; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja1102822

Reference yield:

: 92473-47-7
(3,3-dimethylbutynyl)(phenyl)iodonium tosylate

: 591-50-4
iodobenzene

: 23700-63-2
1-iodo-3,3-dimethylbut-1-yne

: 4250-82-2
(3,3-dimethyl-but-1-ynyl)benzene

Guidance literature:: In dichloromethane; at 15 ℃; for 0.166667h; Product distribution; Quantum yield; Mechanism; Irradiation; var. solvents; other iodonium salts;
DOI:10.1246/cl.1992.2245

Reference yield:

: 917-92-0
3,3-Dimethylbut-1-yne

: 74966-67-9
1,1-diiodo-3,3-dimethyl-butan-2-one

: 23700-63-2
1-iodo-3,3-dimethylbut-1-yne

: 74966-65-7
(E)-1,2-Diiodo-3,3-dimethyl-but-1-ene

Guidance literature:: With iodine; silver nitrate; In methanol; for 1h; Yield given. Title compound not separated from byproducts;
DOI:10.1021/jo01311a020